Category: 64431-96-5

Adding a certain compound to certain chemical reactions, such as: 64431-96-5, 2,2′-(Propane-1,3-diylbis(azanediyl))bis(2-(hydroxymethyl)propane-1,3-diol), can increase the reaction rate and produce products with better performance than those obtained under traditional synthetic methods. Here is a downstream synthesis route of the compound, Safety of 2,2′-(Propane-1,3-diylbis(azanediyl))bis(2-(hydroxymethyl)propane-1,3-diol), blongs to alcohols-buliding-blocks compound. Safety of 2,2′-(Propane-1,3-diylbis(azanediyl))bis(2-(hydroxymethyl)propane-1,3-diol)

[0052]To a solution of bis-ths propane (56.5 g, 0.2 mol) in 200 ml of dry THF in a three-necked round bottom flask with mechanical stir was added trimethylamine (40.52 g, 0.4 mol) at room temperature. The resulting solution was cooled down to 0 C under N2, then a solution of acryloyl chloride (36.2 g, 0.4 mol) in 100 ml of dry THF was added dropwise at 0 C. After the addition was complete, the mixture was allowed to warm to room temperature and continued to stir at room temperature for overnight. The white solid was collected by filtration and washed with THF (3X50 ml). The combined THF filtrate and THF washing solutions were evaporated off to give a residue. The residue was dissolved into 500 ml of chloroform and washed with saturated sodium (0121) bicarbonate aqueous solution (3X100 ml) until no gas generated. The chloroform layer was then dried with sodium sulfate. Sodium sulfate was removed by filtration and the filtrate was evaporated off to give the desired BIS TRIS Propane diacrylamide (BTPDA, Photo Active Co-solvent-1 ) (50.7 g, 65%).

The synthetic route of 64431-96-5 has been constantly updated, and we look forward to future research findings.

Reference:
Patent; HEWLETT-PACKARD DEVELOPMENT COMPANY, L.P.; ZHOU, Zhang-Lin; BAR, Mazi; LANE, Gregg A.; (29 pag.)WO2018/143916; (2018); A1;,
Alcohol – Wikipedia,
Alcohols – Chemistry LibreTexts

The major producers of chemicals have been the Europe, Japan and China. Due to the growing call for a cleaner, greener environment, people will have to find innovative ways to maintain their relevance. Here is a compound 64431-96-5, name is 2,2′-(Propane-1,3-diylbis(azanediyl))bis(2-(hydroxymethyl)propane-1,3-diol). This compound has unique chemical properties. The synthetic route is as follows. Product Details of 64431-96-5

1 was prepared by the self-assembly approach: Na2MoO4¡¤2H2O (1.400g, 6.394mmol) and H6bthmap (0.414g, 1.466mmol) were dissolved in water (30mL, 1665mmol) at room temperature, and then the pH was adjusted to 4.0 with 6mol¡¤L-1 HCl. CoCl2¡¤6H2O (0.237g, 0.996mmol) and Ho(NO3)3¡¤5H2O (0.250g, 0.591mmol) were added, and then the pH was adjusted to 4.0 again with 6mol¡¤L-1 HCl. The reaction solution was stirred at ambient temperature for 30min, kept in the 70C water bath for 30min, filtered and evaporated at room temperature. Colorless block crystals were obtained after three weeks. Yield: ca. 42% (based on Na2MoO4¡¤2H2O). Anal. calcd. (found %) for C22H58Mo8N4Na2O40 (1): C 14.42 (14.63), H 3.19 (3.36), N 3.06 (2.95), Na 2.70 (2.51), Mo 41.74 (41.89). The synthetic method of 2 is similar to that of 1 except that (NH4)6Mo7O24¡¤4H2O (0.800g, 0.647mmol) substituted NaMoO4¡¤2H2O, CoCl2¡¤6H2O was replaced by CuCl2¡¤2H2O (0.400g, 2.346mmol) and the stirring time was added to 45min. Blue block crystals were obtained after two weeks. Yield: ca. 45% (based on (NH4)6Mo7O24¡¤4H2O). Anal. calcd. (found %) for C22H70 Cu2Mo8N10O38 (2): C 13.36 (13.49), H 3.57 (3.75), N 7.08 (6.91), Cu 6.22 (6.43), Mo 38.95 (38.81). Notably, albeit CoCl2¡¤6H2O and Ho(NO3)3¡¤5H2O in the preparation of 1 and Ho(NO3)3¡¤5H2O in the preparation of 2 were used as the starting materials, they can’t be observed in the products. When they were moved away under similar conditions, 1 and 2 can’t be obtained, which suggest that there are the collaborative influences of them and other reaction ingredients during the formation of 1 and 2.

With the rapid development of chemical substances, we look forward to future research findings about 64431-96-5.

Reference:
Article; Li, Hailou; Shao, Bo; Li, Yanyan; Chen, Lijuan; Zhao, Junwei; Inorganic Chemistry Communications; vol. 61; (2015); p. 68 – 72;,
Alcohol – Wikipedia,
Alcohols – Chemistry LibreTexts

The major producers of chemicals have been the Europe, Japan and China. Due to the growing call for a cleaner, greener environment, people will have to find innovative ways to maintain their relevance. Here is a compound 64431-96-5, name is 2,2′-(Propane-1,3-diylbis(azanediyl))bis(2-(hydroxymethyl)propane-1,3-diol). This compound has unique chemical properties. The synthetic route is as follows. 64431-96-5

1 was prepared by the self-assembly approach: Na2MoO4¡¤2H2O (1.400g, 6.394mmol) and H6bthmap (0.414g, 1.466mmol) were dissolved in water (30mL, 1665mmol) at room temperature, and then the pH was adjusted to 4.0 with 6mol¡¤L-1 HCl. CoCl2¡¤6H2O (0.237g, 0.996mmol) and Ho(NO3)3¡¤5H2O (0.250g, 0.591mmol) were added, and then the pH was adjusted to 4.0 again with 6mol¡¤L-1 HCl. The reaction solution was stirred at ambient temperature for 30min, kept in the 70C water bath for 30min, filtered and evaporated at room temperature. Colorless block crystals were obtained after three weeks. Yield: ca. 42% (based on Na2MoO4¡¤2H2O). Anal. calcd. (found %) for C22H58Mo8N4Na2O40 (1): C 14.42 (14.63), H 3.19 (3.36), N 3.06 (2.95), Na 2.70 (2.51), Mo 41.74 (41.89). The synthetic method of 2 is similar to that of 1 except that (NH4)6Mo7O24¡¤4H2O (0.800g, 0.647mmol) substituted NaMoO4¡¤2H2O, CoCl2¡¤6H2O was replaced by CuCl2¡¤2H2O (0.400g, 2.346mmol) and the stirring time was added to 45min. Blue block crystals were obtained after two weeks. Yield: ca. 45% (based on (NH4)6Mo7O24¡¤4H2O). Anal. calcd. (found %) for C22H70 Cu2Mo8N10O38 (2): C 13.36 (13.49), H 3.57 (3.75), N 7.08 (6.91), Cu 6.22 (6.43), Mo 38.95 (38.81). Notably, albeit CoCl2¡¤6H2O and Ho(NO3)3¡¤5H2O in the preparation of 1 and Ho(NO3)3¡¤5H2O in the preparation of 2 were used as the starting materials, they can’t be observed in the products. When they were moved away under similar conditions, 1 and 2 can’t be obtained, which suggest that there are the collaborative influences of them and other reaction ingredients during the formation of 1 and 2.

Statistics shows that 64431-96-5 is playing an increasingly important role. we look forward to future research findings about 2,2′-(Propane-1,3-diylbis(azanediyl))bis(2-(hydroxymethyl)propane-1,3-diol).

Reference:
Article; Li, Hailou; Shao, Bo; Li, Yanyan; Chen, Lijuan; Zhao, Junwei; Inorganic Chemistry Communications; vol. 61; (2015); p. 68 – 72;,
Alcohol – Wikipedia,
Alcohols – Chemistry LibreTexts

Researchers who often do experiments know that organic synthesis is a process of preparing more complex target molecules from simple raw materials through one or more chemical reactions. Generally, it requires fewer steps,and cheap raw materials. 64431-96-5, name is 2,2′-(Propane-1,3-diylbis(azanediyl))bis(2-(hydroxymethyl)propane-1,3-diol). A new synthetic method of this compound is introduced below., 64431-96-5

As shown in Scheme 8, reaction of 2 equivalents of TPO chloride (2) with Bis-tris propane (8) in the presence of K2C03 in acetonitrile under reflux gives water soluble photo initiator VIII.

At the same time, in my other blogs, there are other synthetic methods of this type of compound,64431-96-5, 2,2′-(Propane-1,3-diylbis(azanediyl))bis(2-(hydroxymethyl)propane-1,3-diol), and friends who are interested can also refer to it.

Reference:
Patent; HEWLETT-PACKARD DEVELOPMENT COMPANY, L.P.; ZHOU, Zhang-Lin; (44 pag.)WO2018/143928; (2018); A1;,
Alcohol – Wikipedia,
Alcohols – Chemistry LibreTexts