Category: 4249-72-3

Adding a certain compound to certain chemical reactions, such as: 4249-72-3, 2-Phenoxy-1-phenylethanol, can increase the reaction rate and produce products with better performance than those obtained under traditional synthetic methods. Here is a downstream synthesis route of the compound, Safety of 2-Phenoxy-1-phenylethanol, blongs to alcohols-buliding-blocks compound. Safety of 2-Phenoxy-1-phenylethanol

General procedure: In a typical reaction, 125 ML phosphate buffer (0.2 mol L-1, pH 7),90 ML distilled water, 265 ML AuNPs-GQDs18 (0.72 g L-1, 0.01 mg gold)were mixed. Then, 0.1 mg substrate in 50 ML ethanol was dried at 50 Cin an open bottle. The bottle was sealed after the AuNPs-GQDs18 solutionand 20 ML fresh H2O2 (30 g L-1) was injected into it. The reactionmixture was heated at 75 C for 4 h in a horizonal oscillator. The conversionand yield were determined by HPLC. The catalyst could be recoveredby dialysis (8000-140,000 Da) and reused for 2 times (seeTable S3).

The synthetic route of 4249-72-3 has been constantly updated, and we look forward to future research findings.

Reference:
Article; Zhang, Fangwei; Zhang, Jiali; Guo, Shouwu; Inorganic Chemistry Communications; vol. 104; (2019); p. 105 – 109;,
Alcohol – Wikipedia,
Alcohols – Chemistry LibreTexts

Electric Literature of 4249-72-3, The major producers of chemicals have been the Europe, Japan and China. Due to the growing call for a cleaner, greener environment, people will have to find innovative ways to maintain their relevance. Here is a compound 4249-72-3, name is 2-Phenoxy-1-phenylethanol. This compound has unique chemical properties. The synthetic route is as follows.

General procedure: Lignin model molecule (2-phenoxy-1-phenylethanol) wassynthesized according to the method reported by Rothenberg[9]. Catalytic hydrotreating of 2-phenoxy-1-phenylethanolwas carried out in a 100ml autoclave with Tefon liner.The catalyst (50mg) was added to a solution of 2-phenoxy-1-phenylethanol (150mg) in ethanol (2ml) and H2O(8ml).The autoclave was sealed and purged with H2several times.The reaction was performed at 170C with 2MPa hydrogenpressure for 6h. Then, the reactors were cooled down toroom temperature using an ice bath, and the organic productswere extracted with ethyl acetate (5ml × 2). The organic products mixtures were analyzed by GC and chlorobenzenewas used as an external standard. Identification of mainproducts was based on GC-MS as well as by comparisonwith authentic samples. The product distribution was shownon the mole basis. In consecutive batch tests, the catalystwas recovered by magnets and washed with EtOH for threetimes. The catalyst was recycled into the autoclave with thefeedstream.

While traditionally a conservative industry, chemical producers will need to modernize their PR strategies to stay relevant.we look forward to future research findings about 4249-72-3, 2-Phenoxy-1-phenylethanol.

Reference:
Article; Chen, Bingfeng; Li, Fengbo; Yuan, Guoqing; Catalysis Letters; vol. 147; 11; (2017); p. 2877 – 2885;,
Alcohol – Wikipedia,
Alcohols – Chemistry LibreTexts

Related Products of 4249-72-3 ,Some common heterocyclic compound, 4249-72-3, molecular formula is C14H14O2, its traditional synthetic route has been very mature, but the traditional synthetic route has various shortcomings, such as complicated route, low yield, poor purity, etc., below Introduce a new synthetic route.

The reaction feed is carried out in a glove box.Weigh lignin dimer 5 (0.1 mmol, 21.4 mg),Photocatalyst antimony trichloride (1 mol%), auxiliary tetrabutylammonium chloride (5 mol%),Di-tert-butyl azodicarboxylate (0.1 mmol) and 0.5 mL of acetonitrile were placed in a 10 ml reaction pressure tube. The reaction pressure tube is sealed in a blue light at 420 nm.After stirring for 12 hours, after the lignin dimer 5 is completely converted,Continue to add lignin dimer 5 (0.1 mmol, 21.4 mg) to the reaction.And di-tert-butyl azodicarboxylate (0.1 mmol), each time after the reaction,The conversion and product yield are shown in Figure 3. After the tenth feeding reaction is over,After separation by silica gel column chromatography (ethyl acetate: petroleum ether = 1:5, volume ratio), the product benzaldehyde (84.8 mg, yield 80%)And 1-(phenoxymethyl)-1,2-dicarboxylic acid di-tert-butyl ester-oxime (1)(267.0 mg, yield 79%).

These compound has a wide range of applications. It is believed that with the continuous development of the source of the synthetic route,4249-72-3, its application will become more common.

Reference:
Patent; Jilin University; Zhang Yuetao; He Jianghua; Wang Yinling; (11 pag.)CN110156581; (2019); A;,
Alcohol – Wikipedia,
Alcohols – Chemistry LibreTexts

Adding a certain compound to certain chemical reactions, such as: 4249-72-3, 2-Phenoxy-1-phenylethanol, can increase the reaction rate and produce products with better performance than those obtained under traditional synthetic methods. Here is a downstream synthesis route of the compound, Formula: C14H14O2, blongs to alcohols-buliding-blocks compound. Formula: C14H14O2

2-phenoxy-1-phenylethan-1-ol ((50 gm, 0.236 mmol), TEMPO (7.3 mg, 0.047 mmol), CuCl (4.6 mg, 0.047 mmol), NMI (7.7 mg, 0.94 mmol), bpy (7.3 mg, 0.047 mmol) and MeCN (.93 mL, 0.25 M of substrate) stirred under an air atmosphere (1 atm) at 25 C for 20 h. The reaction mixture was quenched with 1 N HCl and product were extracted with dichloromethane. The organic layer was washed with the water, dried over MgSO4 and concentrated under vacuum. The products were separated by silica-gel column chromatography (EtOAc:hexane 1:20) to produce 2-phenoxy-1-phenylethan-1-ol (48 mg, 0.224 mmol, 95%), 2-phenoxy-1-phenylethan-1-one (2.5 mg, 0.012 mmol, 5%).

At the same time, in my other blogs, there are other synthetic methods of this type of compound,4249-72-3, 2-Phenoxy-1-phenylethanol, and friends who are interested can also refer to it.

Reference:
Article; Patil, Nikhil D.; Yan, Ning; Tetrahedron Letters; vol. 57; 27-28; (2016); p. 3024 – 3028;,
Alcohol – Wikipedia,
Alcohols – Chemistry LibreTexts

Each compound has different characteristics, and only by selecting the characteristics of the compound suitable for a specific situation can the compound be applied on a large scale. 4249-72-3, name is 2-Phenoxy-1-phenylethanol. This compound has unique chemical properties. The synthetic route is as follows. Application In Synthesis of 2-Phenoxy-1-phenylethanol

0.2 mmol of lignin template compound,20mg catalyst,1.5mL of methanol was added to the 25mL inflation tube,After the oxygen was replaced three times, it was reacted in an oil bath at 80 to 120 C for 12 to 24 hours.After the reaction was cooled, the catalyst and the reaction liquid were separated, and the organic phase was evaporated to remove the solvent.The starting materials and yields are shown in the table below.

If you are interested in these compounds, you can also browse my other articles.Thank you for taking the time to read this article. I hope you enjoyed it, 4249-72-3, 2-Phenoxy-1-phenylethanol.

Reference:
Patent; Nanjing University of Science and Technology; Lu Guoping; Sun Kangkang; (6 pag.)CN108821952; (2018); A;,
Alcohol – Wikipedia,
Alcohols – Chemistry LibreTexts

Reference of 4249-72-3, As we all know, there are many different methods for the synthesis of a compound, and people can choose the synthesis method that suits their own laboratory according to the actual situation. 4249-72-3, name is 2-Phenoxy-1-phenylethanol, molecular formula is C14H14O2, The compound is widely used in many fields, so it is necessary to find a new synthetic route. The downstream synthesis method of this compound is introduced below.

General procedure: Lignin model molecule (2-phenoxy-1-phenylethanol) wassynthesized according to the method reported by Rothenberg[9]. Catalytic hydrotreating of 2-phenoxy-1-phenylethanolwas carried out in a 100ml autoclave with Tefon liner.The catalyst (50mg) was added to a solution of 2-phenoxy-1-phenylethanol (150mg) in ethanol (2ml) and H2O(8ml).The autoclave was sealed and purged with H2several times.The reaction was performed at 170C with 2MPa hydrogenpressure for 6h. Then, the reactors were cooled down toroom temperature using an ice bath, and the organic productswere extracted with ethyl acetate (5ml ¡Á 2). The organic products mixtures were analyzed by GC and chlorobenzenewas used as an external standard. Identification of mainproducts was based on GC-MS as well as by comparisonwith authentic samples. The product distribution was shownon the mole basis. In consecutive batch tests, the catalystwas recovered by magnets and washed with EtOH for threetimes. The catalyst was recycled into the autoclave with thefeedstream.

According to the analysis of related databases, 4249-72-3, the application of this compound in the production field has become more and more popular.

Reference:
Article; Chen, Bingfeng; Li, Fengbo; Yuan, Guoqing; Catalysis Letters; vol. 147; 11; (2017); p. 2877 – 2885;,
Alcohol – Wikipedia,
Alcohols – Chemistry LibreTexts