Adding a certain compound to certain chemical reactions, such as: 2277-23-8, 2,3-Dihydroxypropyl decanoate, can increase the reaction rate and produce products with better performance than those obtained under traditional synthetic methods. Here is a downstream synthesis route of the compound, Quality Control of 2,3-Dihydroxypropyl decanoate, blongs to alcohols-buliding-blocks compound. Quality Control of 2,3-Dihydroxypropyl decanoate
Compound 1, 100 mg, compound 2, 76 mg,120 mg of 1-ethyl- (3-dimethylaminopropyl) carbodiimide hydrochloride (EDCI)42 mg of 1-hydroxybenzotriazole (HOBt) was dissolved in 2 ml of THF,The reactants were mixed and replaced with nitrogen three times,After stirring at room temperature for 1 hour.TLC detection (DCM: MeOH = 5: 1), the remaining starting material,The system was concentrated directly and scraped into large plates (DCM: MeOH = 10: 1) to give 51 mg of a light yellow oil.
The synthetic route of 2277-23-8 has been constantly updated, and we look forward to future research findings.
Reference:
Patent; Si Fenke Si Pharmaceutical Research And Development (Tianjin) Co., Ltd.; Yao Qingjia; Wu Simin; Xu Yangjun; (6 pag.)CN106749210; (2017); A;,
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