Nesterova, Oksana V. et al. published their research in Dalton Transactions in 2018 |CAS: 2160-93-2

The Article related to copper iron manganese alkoxo butyldiethanolamine pivalate complex preparation magnetism, oxidation catalyst copper iron manganese alkoxo butyldiethanolamine pivalate, crystal structure copper iron manganese alkoxo butyldiethanolamine pivalate and other aspects.Product Details of 2160-93-2

Nesterova, Oksana V.; Nesterov, Dmytro S.; Vranovicova, Beata; Boca, Roman; Pombeiro, Armando J. L. published an article in 2018, the title of the article was Heterometallic CuIIFeIII and CuIIMnIII alkoxo-bridged complexes revealing a rare hexanuclear M6(μ-X)7(μ3-X)2 molecular core.Product Details of 2160-93-2 And the article contains the following content:

The novel hexanuclear complexes [Cu4Fe2(OH)(Piv)4(tBuDea)4Cl]·0.5CH3CN (1) and [Cu4Mn2(OH)(Piv)4(tBuDea)4Cl] (2) were prepared through one-pot self-assembly reactions of copper powder and iron(II) or manganese(II) chloride with N-tert-butyldiethanolamine (H2tBuDea) and pivalic acid (HPiv) in acetonitrile. Crystallog. studies revealed the uncommon mol. core type M6(μ-X)7(μ3-X)2 in 1 and 2, which can be viewed as a combination of two trimetallic M3(μ-X)2(μ3-X) fragments joined by three bridging atoms. The anal. and classification of the hexanuclear complexes having a M3(μ-X)2(μ3-X) moiety as a core forming fragment using data from the Cambridge Structural Database (CSD) were performed. Variable-temperature (1.8-300 K) magnetic susceptibility measurements of 1 showed a decrease of the effective magnetic moment value at low temperature, indicative of antiferromagnetic coupling between the magnetic centers (JFe-Cu/hc = -6.9 cm-1, JCu-Cu/hc = -4.1 cm-1, JFe-Fe/hc = -24.2 cm-1). Complex 1 acts as a catalyst in the reaction of mild oxidation of cyclohexane with H2O2, showing the yields of products, cyclohexanol and cyclohexanone, up to 17% using pyrazinecarboxylic acid as a promoter. In the oxidation of cis-1,2-dimethylcyclohexane with m-chloroperoxybenzoic acid (m-CPBA), 70% of retention of stereoconfiguration was observed for tertiary alcs. Compound 1 also catalyzes the amidation of cyclohexane with benzamide. In all three catalytic reactions the byproducts were investigated in detail and discussed. The experimental process involved the reaction of 2,2′-(tert-Butylazanediyl)diethanol(cas: 2160-93-2).Product Details of 2160-93-2

The Article related to copper iron manganese alkoxo butyldiethanolamine pivalate complex preparation magnetism, oxidation catalyst copper iron manganese alkoxo butyldiethanolamine pivalate, crystal structure copper iron manganese alkoxo butyldiethanolamine pivalate and other aspects.Product Details of 2160-93-2

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Nesterova, Oksana V. et al. published their research in Inorganic Chemistry in 2018 |CAS: 2160-93-2

The Article related to epr magnetic susceptibility copper n substituted diethanolamine complex, oxidative dehydrogenation cyclohexane amidation copper n substituted diethanolamine complex, crystal structure dinuclear copper n substituted diethanolamine complex preparation and other aspects.Synthetic Route of 2160-93-2

On October 1, 2018, Nesterova, Oksana V.; Nesterov, Dmytro S.; Jezierska, Julia; Pombeiro, Armando J. L.; Ozarowski, Andrew published an article.Synthetic Route of 2160-93-2 The title of the article was Copper(II) Complexes with Bulky N-Substituted Diethanolamines: High-Field Electron Paramagnetic Resonance, Magnetic, and Catalytic Studies in Oxidative Cyclohexane Amidation. And the article contained the following:

The novel coordination compounds [Cu2(HtBuDea)2(OAc)2] (1) and [Cu2(HBuDea)2Cl2]·nH2O (2) have been prepared through the reaction of the resp. copper(II) salts with N-tert-butyldiethanolamine (H2tBuDea, for 1) or N-butyldiethanolamine (H2BuDea, for 2) in methanol solution Crystallog. anal. reveals that, in spite of the common binuclear {Cu2(μ-O)2} core, the supramol. structures of the complexes are drastically different. In 1 binuclear mols. are linked together by H-bonds into 1D chains, while in 2 the neighboring pairs of binuclear mols. are H-bonded, forming tetranuclear aggregates. Variable-temperature (1.8-300 K) magnetic susceptibility measurements of 1 and 2 show a dominant antiferromagnetic behavior. Both complexes were also studied by HF-EPR spectroscopy. While the interaction between Cu(II) centers in 1 can be described by a single coupling constant J = 130.1(3) cm-1 (using H = JS1S2), the crystallog. different {Cu2(μ-O)2} pairs in 2 are expected exchange from ferro- to antiferromagnetic behavior (with J ranging from -32 to 110 cm-1, according to DFT calculations). Complexes 1 and 2 act as catalysts in the amidation of cyclohexane with benzamide, employing tBuOOtBu as oxidant. The maximum achieved conversion of benzamide (20%, after 24 h reaction time) was observed in the 1/tBuOOtBu system. In the cases of tBuOO(O)CPh or tBuOOH oxidants, no significant amidation product was observed, while for tBuOO(O)CPh, the oxidative dehydrogenation of cyclohexane occurred, giving cyclohexene, to afford the allylic ester (cyclohex-2-en-1-yl benzoate) as the main reaction product. The experimental process involved the reaction of 2,2′-(tert-Butylazanediyl)diethanol(cas: 2160-93-2).Synthetic Route of 2160-93-2

The Article related to epr magnetic susceptibility copper n substituted diethanolamine complex, oxidative dehydrogenation cyclohexane amidation copper n substituted diethanolamine complex, crystal structure dinuclear copper n substituted diethanolamine complex preparation and other aspects.Synthetic Route of 2160-93-2

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Krol, Piotr et al. published their research in Colloid and Polymer Science in 2013 |CAS: 2160-93-2

The Article related to modeling surface free energy parameter linear polyurethane coating, additive model of the surface free energy, contact angles, nmr spectroscopy, owens–wendt method, prediction of the surface free energy parameter, synthesis of the polyurethane coatings and other aspects.COA of Formula: C8H19NO2

On March 31, 2013, Krol, Piotr; Lechowicz, Jaromir B.; Krol, Bozena published an article.COA of Formula: C8H19NO2 The title of the article was Modelling the surface free energy parameters of polyurethane coats-part 1. Solvent-based coats obtained from linear polyurethane elastomers. And the article contained the following:

Polyurethane elastomers coating were synthesized by using typical diisocyanates, polyether and polyester polyols and HO-tertiary amines or diols as a chain extenders. Mole fractions of structural fragments (κexp) responsible for the polar interactions within polyurethane chains were calculated by 1H NMR method. Obtained results were confronted with the analogous parameter values (κtheor) calculated on the basis of process stoichiometry, considering the stage of the production of isocyanate prepolymers and reaction of their extension for polyurethanes. Trials of linear correlation between the κexp parameters and surface free energy (SFE) values of studied coatings were presented. SFE values were determined by Owens-Wendt method, using contact angles measured with the goniometric method. Based on achieved results, another empirical models, allowing for prediction the influence of the kind of polyurethane raw materials on SFE values of received coatings were determined It is possible to regulate the SFE in the range millijoules per cubic metre by the selection of appropriate substrates. Use of 2,2,3,3-tetrafluoro-1,4-butanediol as a fluorinated extender of prepolymer chains is essential to obtain coatings with increased hydrophobicity, applied among others as biomaterials-next to diphenylmethane diisocyanate and polyoxyethylene glycol. The experimental process involved the reaction of 2,2′-(tert-Butylazanediyl)diethanol(cas: 2160-93-2).COA of Formula: C8H19NO2

The Article related to modeling surface free energy parameter linear polyurethane coating, additive model of the surface free energy, contact angles, nmr spectroscopy, owens–wendt method, prediction of the surface free energy parameter, synthesis of the polyurethane coatings and other aspects.COA of Formula: C8H19NO2

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Porcheron, Fabien et al. published their research in Environmental Science & Technology in 2011 |CAS: 2160-93-2

The Article related to coal fired power generation flue gas carbon dioxide capture, aqueous amine solution solvent flue gas carbon dioxide capture, high throughput screening apparatus amine carbon dioxide solubility capture, thermodn modeling aqueous amine capture flue gas carbon dioxide and other aspects.HPLC of Formula: 2160-93-2

On March 15, 2011, Porcheron, Fabien; Gibert, Alexandre; Mougin, Pascal; Wender, Aurelie published an article.HPLC of Formula: 2160-93-2 The title of the article was High Throughput Screening of CO2 Solubility in Aqueous Monoamine Solutions. And the article contained the following:

Post-combustion C capture and storage technol. (CCS) is an efficient solution to reduce CO2 emissions at coal-fired power generating facilities. In CCS, an aqueous amine solution is commonly used as a solvent to selectively capture CO2 from flue gas; however, this process generates addnl. cost, mostly from the re-boiler heat duty required to release CO2 from the loaded solvent solution This work presents thermodn. results of CO2 solubility in aqueous amine solutions from a 6-reactor, high through-put screening (HTS) exptl. device. This fully automated device is designed to sequentially inject CO2 into stirred-cell reactors containing the solvent solutions The gas pressure in each reactor is monitored as a function of time; resulting transient pressure curves are transformed into CO2 absorption isotherms. First solubility of monoethanolamine, diethanolamine, and methyldiethanolamine aqueous solutions was measured at 313.15° K. Exptl. results were compared to existing literature data to validate the HTS device. Also, a comprehensive thermodn. model was used to represent CO2 solubility variations in different classes of amine structures at a wide range of thermodn. conditions. This model fitted exptl. data and calculated the cyclic capacity, a key parameter for CO2 process design. Solubility measurements were then performed on a set of 50 monoamines and cyclic capacities were extracted using the thermodn. model, to asses the potential of these mols. to capture CO2. The experimental process involved the reaction of 2,2′-(tert-Butylazanediyl)diethanol(cas: 2160-93-2).HPLC of Formula: 2160-93-2

The Article related to coal fired power generation flue gas carbon dioxide capture, aqueous amine solution solvent flue gas carbon dioxide capture, high throughput screening apparatus amine carbon dioxide solubility capture, thermodn modeling aqueous amine capture flue gas carbon dioxide and other aspects.HPLC of Formula: 2160-93-2

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Kloewer, Frederik et al. published their research in Chemistry – A European Journal in 2009 |CAS: 2160-93-2

The Article related to cobalt pentanuclear cluster azido chloro bridged preparation crystal structure, smm behavior cobalt pentanuclear cluster azido chloro bridged, magnetic property cobalt pentanuclear cluster azido chloro bridged, square pyramid cluster cobalt preparation smm behavior and other aspects.Application In Synthesis of 2,2′-(tert-Butylazanediyl)diethanol

Kloewer, Frederik; Lan, Yanhua; Nehrkorn, Joscha; Waldmann, Oliver; Anson, Christopher E.; Powell, Annie K. published an article in 2009, the title of the article was Modelling the Magnetic Behaviour of Square-Pyramidal CoII5 Aggregates: Tuning SMM Behaviour through Variations in the Ligand Shell.Application In Synthesis of 2,2′-(tert-Butylazanediyl)diethanol And the article contains the following content:

Three new μ4-bridged CoII5 clusters with similar core motifs were synthesized using N-tert-butyldiethanolamine (tbdeaH2) and pivalic acid (piv): [CoII5(μ4-N3)(tbdea)2(μ-piv)4(piv)(MeCN)2]·MeCN (1), [CoII5(μ4-Cl)(Cl)(tbdea)2(μ-piv)4(pivH)2] (2) and [CoII5(μ4-N3)(Cl)(tbdea)2(μ-piv)4(pivH)2] (3). Magnetic measurements were performed for all three compounds While the chloride-bridged cluster 2 does not show an out-of-phase signal, which excludes single-mol. magnet (SMM) behavior, the azide-bridged compounds 1 and 3 show out-of-phase signals as well as frequency dependence of the a.c. susceptibility, as expected for SMMs. Is a SMM with zero-field quantum tunnelling of the magnetization at 1.8 K. Compound 3 is likely a SMM with a blocking temperature well <1.8 K. The authors established a phys. model to fit the χT vs. T and M vs. B curves of the three compounds to reproduce the observed SMM trend. The anal. showed that small changes in the ligand shell modify not only the magnitude of exchange constants, but also affect the J and g matrixes in a nontrivial way. The experimental process involved the reaction of 2,2'-(tert-Butylazanediyl)diethanol(cas: 2160-93-2).Application In Synthesis of 2,2′-(tert-Butylazanediyl)diethanol

The Article related to cobalt pentanuclear cluster azido chloro bridged preparation crystal structure, smm behavior cobalt pentanuclear cluster azido chloro bridged, magnetic property cobalt pentanuclear cluster azido chloro bridged, square pyramid cluster cobalt preparation smm behavior and other aspects.Application In Synthesis of 2,2′-(tert-Butylazanediyl)diethanol

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Femia, Frank J. et al. published their research in Inorganica Chimica Acta in 2000 |CAS: 2160-93-2

The Article related to rhenium oxo thiobisethanolato iminobisethanolato mercaptopyridine mercaptopyrimidine preparation, thioether rhenium oxo mercaptopyridine mercaptopyrimidine preparation, crystal structure rhenium oxo thiobisethanolato iminobisethanolato mercaptopyridine mercaptopyrimidine and other aspects.Reference of 2,2′-(tert-Butylazanediyl)diethanol

On April 30, 2000, Femia, Frank J.; Babich, John W.; Zubieta, Jon published an article.Reference of 2,2′-(tert-Butylazanediyl)diethanol The title of the article was Structural systematics of the {ReO}3+ core with ‘3+2’ ligand donor sets. And the article contained the following:

The reactions of [ReOCl3(PPh3)2] with the appropriate tridentate and bidentate ligands provide a facile route for the synthesis of a diverse family of compounds of the {Re(V)O}3+ core with a ‘3+2′ ligand set. The structural prototype for the series is [ReO{OCH2CH2SCH2CH2O}{OCH2CH2SCH2CH2OH}] (1) which exhibits distorted octahedral geometry, defined by the two oxygen and sulfur donors of the tridentate ligand in a facial arrangement, the oxygen and sulfur donors of the bidentate ligand, and the oxo-donor. Compounds 2-5 are variants [ReO(OCH2CH2SCH2CH2O)(S and N)] where S and N is a bidentate ligand of the mercaptopyridine or mercaptopyrimidine class. Similarly, compounds 6-17 are [ReO(OCH2CH2NRCH2CH2O)(S and N)] with the same bidentate ligands as for 2-5 and R = Me, Et, Bu, and t-Bu. The experimental process involved the reaction of 2,2’-(tert-Butylazanediyl)diethanol(cas: 2160-93-2).Reference of 2,2′-(tert-Butylazanediyl)diethanol

The Article related to rhenium oxo thiobisethanolato iminobisethanolato mercaptopyridine mercaptopyrimidine preparation, thioether rhenium oxo mercaptopyridine mercaptopyrimidine preparation, crystal structure rhenium oxo thiobisethanolato iminobisethanolato mercaptopyridine mercaptopyrimidine and other aspects.Reference of 2,2′-(tert-Butylazanediyl)diethanol

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Chen, Sihuai et al. published their research in Dalton Transactions in 2018 |CAS: 2160-93-2

The Article related to dodecanuclear chromium rare earth metal dithanolamine benzoate cluster preparation, crystal structure dodecanuclear chromium rare earth metal cluster, magnetic property dodecanuclear chromium rare earth metal cluster, thermal stability dodecanuclear chromium rare earth metal cluster and other aspects.Name: 2,2′-(tert-Butylazanediyl)diethanol

Chen, Sihuai; Mereacre, Valeriu; Zhao, Zhiying; Zhang, Wanwan; Zhang, Mengsi; He, Zhangzhen published an article in 2018, the title of the article was Targeted replacement: systematic studies of dodecanuclear {MIII6LnIII6} coordination clusters (M = Cr, Co; Ln = Dy, Y).Name: 2,2′-(tert-Butylazanediyl)diethanol And the article contains the following content:

Three dodecanuclear 3d-4f coordination clusters, [CrIII6LnIII6(μ3-OH)8(tbdea)6(C6H5COO)16]·2H2O (Ln = Dy (1), Y (2)) and [CoIII6DyIII6(μ3-OH)8(nbdea)6(m-CH3C6H4COO)16]·2H2O·2CH3CN (3), have been synthesized under solvothermal conditions and characterized. Single-crystal x-ray diffraction anal. revealed that all three compounds possess an analogous {M6IIILnIII6} core (M = Cr, Co; Ln = Dy, Y) and dc magnetic susceptibility studies indicated that the magnetic exchange couplings between DyIII ions are dominant antiferromagnetic, while the CrIII-DyIII interactions are weakly ferromagnetic. Furthermore, the ac magnetic susceptibility measurements showed that both CrIII6DyIII6 compound 1 and CoIIi6DyIII6 compound 3 containing highly anisotropic DyIII ions displayed single-mol. magnetic (SMM) behavior with the energy barrier Ueff increasing from 12.8 K (for 1) to 20.8 K (for 3), indicating that weak 3d-4f exchange couplings enhance the QTM and reduce the energy barrier. The experimental process involved the reaction of 2,2′-(tert-Butylazanediyl)diethanol(cas: 2160-93-2).Name: 2,2′-(tert-Butylazanediyl)diethanol

The Article related to dodecanuclear chromium rare earth metal dithanolamine benzoate cluster preparation, crystal structure dodecanuclear chromium rare earth metal cluster, magnetic property dodecanuclear chromium rare earth metal cluster, thermal stability dodecanuclear chromium rare earth metal cluster and other aspects.Name: 2,2′-(tert-Butylazanediyl)diethanol

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Prakash, Raju et al. published their research in Angewandte Chemie, International Edition in 2006 |CAS: 2160-93-2

The Article related to iron diethanolamine octanuclear complex preparation structure, calcium capped iron heterodecanuclear complex preparation structure, crystal structure iron diethanolamine polynuclear complex with without calcium, electrochem iron diethanolamine oligonuclear complex with without calcium and other aspects.Synthetic Route of 2160-93-2

On September 4, 2006, Prakash, Raju; Saalfrank, Rolf W.; Maid, Harald; Scheurer, Andreas; Heinemann, Frank W.; Trautwein, Alfred X.; Bottger, Lars H. published an article.Synthetic Route of 2160-93-2 The title of the article was Synthesis and redox properties of mixed-valent octanuclear iron defective hexacubanes and a (CaCl)-capped body-centered six-sided iron(III) polyhedron. And the article contained the following:

Three new oligo nuclear complexes [FeII4FeII4(L3)6Cl4O2] (1; H2L3 = N-(tert-butyl)-diethanolamine), [FeII2FeIII6(L3)6Cl6O2] and Na3[FeIII9(L3)8Cl4O6(CaCl)2] self-assemble from N-tert-Bu-diethanolamine and mixtures of Fe(II) and Fe(III) ions. Depending on the reaction conditions, a compact or linear defective hexacubane, or a body-centered six-sided Fe(III) polyhedron is formed. The experimental process involved the reaction of 2,2′-(tert-Butylazanediyl)diethanol(cas: 2160-93-2).Synthetic Route of 2160-93-2

The Article related to iron diethanolamine octanuclear complex preparation structure, calcium capped iron heterodecanuclear complex preparation structure, crystal structure iron diethanolamine polynuclear complex with without calcium, electrochem iron diethanolamine oligonuclear complex with without calcium and other aspects.Synthetic Route of 2160-93-2

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Nesterova, Oksana V. et al. published their research in CrystEngComm in 2014 |CAS: 2160-93-2

The Article related to copper pivalate paddlewheel diethanolamine bridge coordination polymer preparation, crystal structure copper pivalate paddlewheel diethanolamine bridge coordination polymer, magnetic exchange copper pivalate paddlewheel diethanolamine bridge coordination polymer, hydrocarboxylation catalyst copper pivalate paddlewheel diethanolamine bridge coordination polymer and other aspects.Related Products of 2160-93-2

Nesterova, Oksana V.; Kirillova, Marina V.; Guedes da Silva, M. Fatima C.; Boca, Roman; Pombeiro, Armando J. L. published an article in 2014, the title of the article was How to force a classical chelating ligand to a metal non-chelating bridge: the observation of a rare coordination mode of diethanolamine in the 1D complex {[Cu2(Piv)4(H3tBuDea)](Piv)}n.Related Products of 2160-93-2 And the article contains the following content:

The novel chain coordination polymer {[Cu2(Piv)4(H3tBuDea)](Piv)}n (1) was prepared through the self-assembly reaction of copper(II) nitrate with pivalic acid (HPiv) and N-tert-butyldiethanolamine (H2tBuDea) in MeCN solution Crystallog. anal. revealed the extremely rare nonchelating bridging coordination mode of diethanolamine ligand in 1, observed for the first time in transition metal complexes, as well as in complexes of diethanolamine having a noncoordinating aliphatic group at the N atom. Possible reasons for such a coordination and anal. of the main coordination modes of diethanolamine-based ligands are discussed. Variable-temperature (1.8-300 K) magnetic susceptibility measurements showed that 1 represents a rare example of dicopper(II) tetracarboxylate that is a diamagnetic solid at room temperature This behavior is compared with literature examples and discussed from DFT calculations Also, 1 acts as an efficient catalyst for the mild hydrocarboxylation of linear and cyclic C5-C8 alkanes into the corresponding carboxylic acids. The experimental process involved the reaction of 2,2′-(tert-Butylazanediyl)diethanol(cas: 2160-93-2).Related Products of 2160-93-2

The Article related to copper pivalate paddlewheel diethanolamine bridge coordination polymer preparation, crystal structure copper pivalate paddlewheel diethanolamine bridge coordination polymer, magnetic exchange copper pivalate paddlewheel diethanolamine bridge coordination polymer, hydrocarboxylation catalyst copper pivalate paddlewheel diethanolamine bridge coordination polymer and other aspects.Related Products of 2160-93-2

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Flinker, Mathias et al. published their research in Angewandte Chemie, International Edition in 2017 |CAS: 2160-93-2

The Article related to chemoselective hydrogenation deuterium exchange carbonyl reduction diboron diethanolamine complex, diboron aminodiol aminotriol complex preparation reductant hydrogen generation, reduction water hydrogen diboron aminodiol aminotriol complex reductant, alkene alkyne chemoselective hydrogenation water hydrogen source diboron and other aspects.Recommanded Product: 2160-93-2

Flinker, Mathias; Yin, Hongfei; Juhl, Rene W.; Eikeland, Espen Z.; Overgaard, Jacob; Nielsen, Dennis U.; Skrydstrup, Troels published an article in 2017, the title of the article was Efficient Water Reduction with sp3-sp3 Diboron(4) Compounds: Application to Hydrogenations, H-D Exchange Reactions, and Carbonyl Reductions.Recommanded Product: 2160-93-2 And the article contains the following content:

Diboron complexes with aminodiols and aminotriols such as I were prepared or generated in situ from (HO)2BB(OH)2; the diboron compounds reduced H2O or D2O to yield H2 or D2 which was used for chemoselective alkene and stereoselective diaryl alkyne hydrogenation, deuterium exchanges, and aldehyde and ketone reductions to alcs. in a two-chamber reactor. The experimental process involved the reaction of 2,2′-(tert-Butylazanediyl)diethanol(cas: 2160-93-2).Recommanded Product: 2160-93-2

The Article related to chemoselective hydrogenation deuterium exchange carbonyl reduction diboron diethanolamine complex, diboron aminodiol aminotriol complex preparation reductant hydrogen generation, reduction water hydrogen diboron aminodiol aminotriol complex reductant, alkene alkyne chemoselective hydrogenation water hydrogen source diboron and other aspects.Recommanded Product: 2160-93-2

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