Category: 13826-35-2

Related Products of 13826-35-2, The transformation of simple hydrocarbons into more complex and valuable products via catalytic C–H bond functionalisation has revolutionised modern synthetic chemistry. 13826-35-2, Name is (3-Phenoxyphenyl)methanol, SMILES is OCC1=CC(OC2=CC=CC=C2)=CC=C1, belongs to alcohols-buliding-blocks compound. In a article, author is Jimenez-Murcia, Susana, introduce new discover of the category.

Objectives: Tobacco smoking and gambling disorder (GD) often co-occur. However, few studies have assessed the extent to which cigarette smoking may serve to classify and/or better define GD behaviour profiles. Methods: Among a large sample of n = 3,652 consecutive treatment-seeking patients with GD (91% men). Smokers were compared to non-smokers across different sociodemographic, clinical, psychopathological and personality variables. The effect sizes for the means and the proportion differences between the groups were estimated. An evaluation of the smoking changes over the last 15 years was also performed. Results: From the total sample, 62.4% of gamblers reported tobacco use. A decreasing linear trend in tobacco use was observed within the studied period, women having a more irregular pattern. The use of tobacco was linked to the use of alcohol and other illegal drugs. Gamblers who smoke, as compared to those who don’t, presented lower education levels, lower social position indexes and active employment. They were younger, with an earlier age of onset, shorter duration of the gambling behavior, higher GD severity, more psychological symptoms, higher scores in novelty seeking and lower scores in reward dependence, self-directedness and self-transcendence. Conclusions: Gamblers seeking treatment who smoke display particular social, clinical, psychological, temperamental and character features different from non-smoking gamblers, suggesting that the presence or absence of comorbid smoking condition in GD should always be considered when developing an optimal treatment, as gamblers who smoke might need treatment strategies different from non-smoking gamblers.

Related Products of 13826-35-2, Enzymes are biological catalysts that produce large increases in reaction rates and tend to be specific for certain reactants and products. I hope my blog about 13826-35-2 is helpful to your research.

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Electric Literature of 13826-35-2, Adding some certain compound to certain chemical reactions, such as: 13826-35-2, name is (3-Phenoxyphenyl)methanol,molecular formula is C13H12O2, can increase the reaction rate and produce products with better performance than those obtained under traditional synthetic methods. Here is a downstream synthesis route of the compound 13826-35-2.

General procedure: General procedure for the one-pot tandem oxidation-Wittig reaction To a flask containing BaMnO4 (1.2 mmol, 300 mg)and the alcohol (1 mmol) in CH3CN (5 mL) were added PPh3(1.2 mmol, 315 mg) and ethyl bromoacetate (1.2 mmol, 0.13 mL) and the mixturewas stirred at 80 C for 24 h. Then the obtained mixture was filtered and theresulting solution was subjected to column chromatography using n-hexane/ethylacetate to isolate the pure products in 78-93% isolated yields with highstereoselectivity.

In the field of chemistry, the synthetic routes of compounds are constantly being developed and updated. I will also mention this compound in other articles. 13826-35-2, (3-Phenoxyphenyl)methanol, other downstream synthetic routes, hurry up and to see.

Reference:
Article; Gholinejad, Mohammad; Firouzabadi, Habib; Bahrami, Maedeh; Najera, Carmen; Tetrahedron Letters; vol. 57; 33; (2016); p. 3773 – 3775;,
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Reference of 13826-35-2, Adding some certain compound to certain chemical reactions, such as: 13826-35-2, name is (3-Phenoxyphenyl)methanol,molecular formula is C13H12O2, can increase the reaction rate and produce products with better performance than those obtained under traditional synthetic methods. Here is a downstream synthesis route of the compound 13826-35-2.

To a solution of triphenyl phosphine (4.52 g; 17.2 mmol) and 3-phenoxybenzyl alcohol (3.44 g; 17.2 mmol) in THF (20 mL) kept in an ice bath was added a solution of 1a (4.61 g; 17.2 mmol) and diisopropyl azodicarboxylate (95%, 3.66 g; 17.2 mmol) in THF (20 mL). The reaction mixture was stirred at 0 C for 2 h and monitored by TLC. The solvent was removed on the rotary evaporator, leaving a yellow oil which was purified by flash chromatography (silica gel/ethyl acetate/hexane) to yield a white solid (6.33 g; 82% yield), mp 75-77 C. 1H NMR (CDCl3): delta 1.49 (s, 9H), 3.65 (d, 2H), 3.72 (s, 3H), 4.79 (s, 2H), 4.77 (t, J = 13.6 Hz, 1H), 6.90-7.03 (m, 4H), 7.10 (d, 2H), 7.30-7.39 (m, 3H).

In the field of chemistry, the synthetic routes of compounds are constantly being developed and updated. I will also mention this compound in other articles. 13826-35-2, (3-Phenoxyphenyl)methanol, other downstream synthetic routes, hurry up and to see.

Reference:
Article; Dou, Dengfeng; Tiew, Kok-Chuan; Mandadapu, Sivakoteswara Rao; Gunnam, Mallikarjuna Reddy; Alliston, Kevin R.; Kim, Yunjeong; Chang, Kyeong-Ok; Groutas, William C.; Bioorganic and Medicinal Chemistry; vol. 20; 6; (2012); p. 2111 – 2118;,
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Application of 13826-35-2, Adding some certain compound to certain chemical reactions, such as: 13826-35-2, name is (3-Phenoxyphenyl)methanol,molecular formula is C13H12O2, can increase the reaction rate and produce products with better performance than those obtained under traditional synthetic methods. Here is a downstream synthesis route of the compound 13826-35-2.

General procedure: A typical reaction was carried out as follows: benzyl alcohol (1 equiv), Oxone (0.88 equiv), and PTC (1.5 equiv) were dissolved in 3 mL of chloroform in a 10-mL glass reactor. The mixture was stirred for 8 h, and the substrate conversion and product formation were monitored by GLC. The products were identified by comparing with authentic samples using GC or GC/MS analysis.

In the field of chemistry, the synthetic routes of compounds are constantly being developed and updated. I will also mention this compound in other articles. 13826-35-2, (3-Phenoxyphenyl)methanol, other downstream synthetic routes, hurry up and to see.

Reference:
Article; An, X. Q.; Kang, M.; Ma, H. C.; Yang, Y. X.; Yang, Z. W.; Zeng, W.; Russian Journal of Organic Chemistry; vol. 56; 3; (2020); p. 521 – 523;,
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Researchers who often do experiments know that organic synthesis is a process of preparing more complex target molecules from simple raw materials through one or more chemical reactions. Generally, it requires fewer steps,and cheap raw materials. 13826-35-2, name is (3-Phenoxyphenyl)methanol. A new synthetic method of this compound is introduced below., HPLC of Formula: C13H12O2

Example 16 – (3-Phenoxyphenyl)methyl 3-[(Z)-2-chloro-3,3,3-trifluoro-prop-1-enyl]-2,2- dimethyl-cyclopropanecarboxylate 13 A solution of 3-[(Z)-2-chloro-3,3,3-trifluoro-prop-1-enyl]-2,2-dimethyl-cyclopropanecarbonyl chloride (242mg, 1.1 eq) in toluene (6ml_) was added dropwise to a solution of (3- phenoxyphenyl)methanol (170mg, 1 eq) and pyridine (68muIota_, 1 eq) in toluene (6ml_). The reaction mixture was stirred overnight at room temperature after which time TLC analysis showed the reaction had gone to completion. The reaction mixture was diluted with ethyl acetate (15ml_) and washed with water (2 x 10ml_) and brine (10ml_) before being dried over MgS04 and the solvent removed in vacuo. The residue was purified by flash chromatography (solvent 9: 1 hexane/ethyl acetate) to afford the product as a clear oil (262mg, 73 %). 1 H NMR deltaEta (CDCIs, 300 MHz): 7.25 (m, 4H), 6.93(m, 6H), 5.00 (dd, J= 15.6, 3.3 Hz, 2H), 2.10 (t, J= 8.4Hz, 1 H), 1.95 (d, J= 8.4Hz, 1 H), 1.22 (s, 3H), 1.20 (s, 3H); ESI-MS 447.1 [MNa]+.

If you are interested in these compounds, you can also browse my other articles.Thank you for taking the time to read this article. I hope you enjoyed it, 13826-35-2, (3-Phenoxyphenyl)methanol.

Reference:
Patent; REDX PHARMA LIMITED; THOMPSON, William; JACKSON, Peter; LINDSAY, Derek; SCREEN, Thomas; MOLTON, Benjamin; URCH, Christopher; WO2013/136073; (2013); A1;,
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Adding a certain compound to certain chemical reactions, such as: 13826-35-2, (3-Phenoxyphenyl)methanol, can increase the reaction rate and produce products with better performance than those obtained under traditional synthetic methods. Here is a downstream synthesis route of the compound, name: (3-Phenoxyphenyl)methanol, blongs to alcohols-buliding-blocks compound. name: (3-Phenoxyphenyl)methanol

In 1000ml four-necked flask (equipped with lye absorption device) was added 500g of dichloromethane, stirring was started to continue the addition of 100g m-phenoxybenzyl alcohol and 30g of tetramethylethylenediamine.Cooling to -35 C, began to drop prepared 70g of thionyl chloride and methylene chloride solution. During the dropwise addition temperature was controlled at -45 C. After the addition was completed at -45 heat 4h. After that, the reaction solution was pouredInto 1000ml of water, stirring, phase separation, the organic phase were washed with 600ml of water, phase separation. The organic phase was desolvated to 100 C under atmospheric pressure and the solvent methylene chloride was recovered. Then decompression (vacuum degree 0.097MP) fractionation, intermediates chloroacenesulfonic acid phenoxybenzyl 127g. Purity 99%, yield 90%.

The synthetic route of 13826-35-2 has been constantly updated, and we look forward to future research findings.

Reference:
Patent; Tianjin Jinlvbao Pesticide To Make Co., Ltd.; Wang Baojun; Cui Weizhong; Lu Sen; (8 pag.)CN106495994; (2017); A;,
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In the next few decades, the world population will flourish. As the population grows rapidly and people all over the world use more and more resources, all industries must consider their environmental impact. 13826-35-2, name is (3-Phenoxyphenyl)methanol, the common compound, a new synthetic route is introduced below. Recommanded Product: (3-Phenoxyphenyl)methanol

(a) 3-Phenoxybenzaldehyde Chromium trioxide (3.00 g.) was added to a stirred solution of pyridine (4.75 g.) in dry methylene chloride (75 ml.), and stirring was continued for a further 15 minutes. 3-Phenoxybenzyl alcohol (1 g.) in methylene chloride (5 ml.) was added, the mixture stirred for a further 15 minutes, decanted and the residue washed with diethyl ether (100 ml.). The filtrate was washed with 5% sodium hydroxide solution (3*50 ml), 2.5 NHCl (50 ml.) and 5% sodium carbonate solution (50 ml.) and dried over Na2 SO4 to give 3-phenoxy-benzaldehyde. Alternatively the alcohol can be oxidized using Jones’ reagent, a similar yield of aldehyde being obtained.

The synthetic route of 13826-35-2 has been constantly updated, and we look forward to future research findings.

Reference:
Patent; National Research Development Corporation; US4464391; (1984); A;,
Alcohol – Wikipedia,
Alcohols – Chemistry LibreTexts

Adding a certain compound to certain chemical reactions, such as: 13826-35-2, (3-Phenoxyphenyl)methanol, can increase the reaction rate and produce products with better performance than those obtained under traditional synthetic methods. Here is a downstream synthesis route of the compound, 13826-35-2, blongs to alcohols-buliding-blocks compound. Recommanded Product: 13826-35-2

General procedure: 4-Phenylphenol 2 (34.0mg, 0.2mmol) and cesium carbonate (97.7mg, 0.3mmol) were weighed to a sealed Schlenk (25mL) under Ar atmosphere. Pentafluorobenzene 1a (50.4mg, 0.3mmol) and DMSO (2.0mL) were added to the sealed Schlenk via syringe at room temperature respectively. The mixture was stirred at room temperature until the completion of the reaction (by TLC). Water (5mL) was added and the mixture was extracted with ethyl acetate (3×10mL). The organic extracts were combined, dried with anhydrous magnesium sulfate and then concentrated in vacuo. The residue was purified on silica gel to afford the product 3o (54.1mg, 85% yield).

These compound has a wide range of applications. It is believed that with the continuous development of the source of the synthetic route,13826-35-2, its application will become more common.

Reference:
Article; Liu, Cuibo; Cao, Liming; Yin, Xuguang; Xu, Haolan; Zhang, Bin; Journal of Fluorine Chemistry; vol. 156; (2013); p. 51 – 60;,
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With the rapid development and complex challenges of chemical substances, the synthesis of new drugs is usually one of the most effective ways to increase yield.13826-35-2, name is (3-Phenoxyphenyl)methanol, molecular formula is C13H12O2, molecular weight is 200.23, as common compound, the synthetic route is as follows.Product Details of 13826-35-2

3- (2-hydroxyphenyl) propionic acid methyl (149.8 mg, 0.831 mmol), 3- phenoxybenzyl alcohol (118.2 mg, 0.590 mmol), triphenylphosphine (198.1 mg, 0.755 mmol) in toluene (5 of 5 mL) solution of , DEAD (2M solution in toluene, 374.6muL, 0.749 mmol) was added dropwise at room temperature and stirred for 3 hours at 70 C.. The solvent of the reaction mixture was evaporated, and the residue was purified by column chromatography (hexane: ethyl acetate = 15: 1) to give the title compound (200.2mg, 0.552 mmol, 94%, yellow oil)

At the same time, in my other blogs, there are other synthetic methods of this type of compound,13826-35-2, (3-Phenoxyphenyl)methanol, and friends who are interested can also refer to it.

Reference:
Patent; THE UNIVERSITY OF TOKYO; TOHOKU UNIVERSITY; OHWADA, TOMOHIKO; NAKAMURA, SHO; JUNG, SEJIN; OTANI, YUKO; SAYAMA, MISA; AOKI, JUNKEN; (80 pag.)JP2016/17036; (2016); A;,
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As we all know, there are many different methods for the synthesis of a compound, and people can choose the synthesis method that suits their own laboratory according to the actual situation. 13826-35-2, name is (3-Phenoxyphenyl)methanol, molecular formula is C13H12O2, The compound is widely used in many fields, so it is necessary to find a new synthetic route. The downstream synthesis method of this compound is introduced below. Formula: C13H12O2

first step: A solution of IV-1 (3-phenoxyphenyl) methanol (0.5 g, 2.5 mmol) obtained in the previous step was dissolved in 30 ml of dichloromethane, and 20 ml of SOCl2 was added to 1 ml of DMF as a catalyst,25 C for 2 hours, After the TLC detection reaction was complete, the reaction solution was evaporated under reduced pressure to give excess SOCl2 to give a pale yellow oil IV-2 which was used directly in the next step.

With the rapid development of chemical substances, we look forward to future research findings about 13826-35-2.

Reference:
Patent; China Pharmaceutical University; Huang Wenlong; Qian Hai; Liu Chunxia; Li Zheng; Yang Jianyong; Bi Xinzhou; Cai Xingguang; (20 pag.)CN107162913; (2017); A;,
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