Mao, Mengmei;Zhang, Le;Yao, Hanlin;Wan, Li;Xin, Zhong published 《Development and Scale-up of the Rapid Synthesis of Triphenyl Phosphites in Continuous Flow》. The research results were published in《ACS Omega》 in 2020.SDS of cas: 80-46-6 The article conveys some information:
A novel method for the synthesis of tri-Ph phosphite and its derivatives was developed in continuous flow. With a total residence time of 20 s, the target product was prepared in a microreactor, and the reaction time was significantly shortened compared with standard single batch reaction conditions. The reaction of various substrates gave the corresponding products in good to excellent yields under optimized conditions. The reactants could be employed in a stoichiometric ratio, making the reaction more efficient, economical, and environmentally friendly. Scale-up apparatus was designed and assembled, and the kilogram-scale production (up to 18.4 kg/h) of tris(2,4-di-tert-butylphenyl) phosphite was achieved in 88% yield. PCl3. And 4-tert-Amylphenol (cas: 80-46-6) was used in the research process.
4-tert-acylphenol (cas:80-46-6) contains hydroxyl group.Some low molecular weight alcohols of industrial importance are produced by the addition of water to alkenes. Ethanol, isopropanol, 2-butanol, and tert-butanol are produced by this general method. SDS of cas: 80-46-6
Reference:
Alcohol – Wikipedia,
Alcohols – Chemistry LibreTexts