Related Products of 110-73-6 ,Some common heterocyclic compound, 110-73-6, molecular formula is C4H11NO, its traditional synthetic route has been very mature, but the traditional synthetic route has various shortcomings, such as complicated route, low yield, poor purity, etc., below Introduce a new synthetic route.
Reference Synthetic Example 19 tert-Butyl ethyl(2-hydroxyethyl)carbamate To a mixture of 2-(ethylamino)ethanol (8.91 g) and ethyl acetate (100 mL) was added di-tert-butyl dicarbonate (21.8 g) under ice-cooling. The reaction mixture was stirred at room temperature for 3 days, and washed with saturated brine, then, dried over anhydrous magnesium sulfate. The solution was concentrated under reduced pressure to give title compound as colorless oil (19.0 g). 1H-NMR (CDCl3): 1.11 (3H, t, J=7.0Hz), 1.47(9H,s), 3. 27 (2H, q, J=7. 0Hz), 3. 37 (2H, t, J=5.2Hz), 3. 73 (2H, q, J=5. 2Hz).
In the field of chemistry, the synthetic routes of compounds are constantly being developed and updated. I will also mention this compound in other articles. 110-73-6, 2-(Ethylamino)ethanol, other downstream synthetic routes, hurry up and to see.
Reference:
Patent; Takeda Pharmaceutical Company Limited; EP1602362; (2005); A1;,
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