Synthetic Route of 92409-15-9, The major producers of chemicals have been the Europe, Japan and China. Due to the growing call for a cleaner, greener environment, people will have to find innovative ways to maintain their relevance. Here is a compound 92409-15-9, name is 2-(2-Methoxyphenoxy)-1-(4-methoxyphenyl)propane-1,3-diol. This compound has unique chemical properties. The synthetic route is as follows.
1 part by weight of the compound2- (2-methoxyphenoxy) -1- (4-methoxyphenyl) -1-hydroxy-3-propanol and 1.8 parts by weightAl (NO3) 3 was added to 30 parts by weight of methanol,Set the microwave reactor power of 50W,Microwave frequency of 2450MHz, microwave-assisted heating at 80 for 40min.After completion of the reaction, the reaction was quenched with cold water immediately,The reaction solution was extracted with ethyl acetate,Take organic phase spin dry,Followed by further separation and purification by silica gel column chromatography,The mobile phase of ethyl acetate and n-hexane volume ratio of 1: 1, evaporated to dry the solvent that methylation products.
According to the analysis of related databases, 92409-15-9, the application of this compound in the production field has become more and more popular.
Reference:
Patent; South China University of Technology; Qiu, Xueqing; Ouyang, Xinping; Zhu, Guodian; Chen, Cheng; Jin, Dongxue; Zhao, Ying; (10 pag.)CN106117021; (2016); A;,
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