Researchers who often do experiments know that organic synthesis is a process of preparing more complex target molecules from simple raw materials through one or more chemical reactions. Generally, it requires fewer steps,and cheap raw materials. 81156-68-5, name is 2,4-Dichlorophenethyl alcohol. A new synthetic method of this compound is introduced below., name: 2,4-Dichlorophenethyl alcohol
(i) Toluene-4-sulfonic acid 2-(2,4-dichloro-phenyl)-ethyl ester This compound was prepared using a procedure analogous to that described for the preparation of Example 169 (i), using 2-(2,4-dichloro-phenyl)-ethanol as the starting material. The compound was recrystallized from n-heptane/ethyl acetate. Yield: 7.12 g MS (Cl+): m/e=345, chloro pattern.
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Reference:
Patent; Nazare, Marc; Essrich, Melanie; Will, David William; Matter, Hans; Ritter, Kurt; Wehner, Volkmar; US2003/199689; (2003); A1;,
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