Reference of 54410-90-1 ,Some common heterocyclic compound, 54410-90-1, molecular formula is C11H22O, its traditional synthetic route has been very mature, but the traditional synthetic route has various shortcomings, such as complicated route, low yield, poor purity, etc., below Introduce a new synthetic route.
General procedure: The compound (T-19) (5.00 g), the compound (T-18) (8.29 g), DMAP (1.0 g) and methylene chloride (80 ml) were placed in a reactor and cooled to 0 C.A solution of DCC (5.00 g) in dichloromethane (40 ml) was slowly added dropwise thereto, returned to room temperature and stirred for 12 hours.After the insolubles were separated, the reaction mixture was poured into water and the aqueous layer was extracted with dichloromethane.The organic layer formed simultaneously with water washing was dried over anhydrous magnesium sulfate.The solution was concentrated under reduced pressure and the residue was purified by silica gel chromatography (volume ratio, heptane: toluene = 1: 1) to obtain compound (T-20) (8.66 g; 75%).
In the field of chemistry, the synthetic routes of compounds are constantly being developed and updated. I will also mention this compound in other articles. 54410-90-1, 4-Pentylcyclohexanol, other downstream synthetic routes, hurry up and to see.
Reference:
Patent; Jieenzhi Co., Ltd.; Jieenzhi Petrochemical Co., Ltd.; Tian Zhongyuzhi; Shi Yekuangyi; Jin Tengshishang; Di Tianhekuan; (145 pag.)CN107108457; (2017); A;,
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