Recently I am researching about SOLID-PHASE SYNTHESES; ETHYL 2-CYANO-2-(2-NITROBENZENESULFONYLOXYIMINO)ACETATE; UNSYMMETRICAL UREAS; INHIBITORS; PEPTIDE; REAGENT; DESIGN; KINASE; ACIDS, Saw an article supported by the Department of Biotechnology, Govt. of IndiaDepartment of Biotechnology (DBT) India [BT/PR16164/NER/95/88/2015, BT/COE/34/SP28408/2018]; DSTDepartment of Science & Technology (India); IITG. Published in WILEY-V C H VERLAG GMBH in WEINHEIM ,Authors: Kalita, T; Dev, D; Mondal, S; Giri, RS; Mandal, B. The CAS is 105-13-5. Through research, I have a further understanding and discovery of (4-Methoxyphenyl)methanol. SDS of cas: 105-13-5
Direct conversion of carboxylic acids to ureas, carbamates, and thiocarbamates in a single pot via Curtius rearrangement is accomplished. One recently established coupling reagent, Ethyl-2-cyano-2-(2-nitrophenylsulfonyloximino)acetate (ortho-NosylOXY, I), is successfully used for the racemization free synthesis of ureas, di-peptidyl ureas, and carbamates with moderate to good yield (82-69%). This single-pot hassle-free procedure works with a diverse range of N-protecting groups Fmoc, Boc, and Cbz. Various amine, including aromatic, methyl esters of amino acids, t-butylamine, alcohols, and thiols, are used as nucleophiles. A detailed NMR-based mechanism study is incorporated here. Racemization suppression, easy removal of by-products, and less waste generation make this methodology useful.
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Reference:
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