Related Products of 3513-81-3, Adding some certain compound to certain chemical reactions, such as: 3513-81-3, name is 2-Methylenepropane-1,3-diol,molecular formula is C4H8O2, can increase the reaction rate and produce products with better performance than those obtained under traditional synthetic methods. Here is a downstream synthesis route of the compound 3513-81-3.
To a solution of 2-methylene-1, 3-propane diol (5.28g, 0.06 mmol) and di-tert-butyl dicarbonate (35 g, 0.16 mol) in 150 ml of dichloromethane was added 6N NaOH (70 ml) and tetrabutylammoniahydrogensulfate (3.4 g, 10 mmol). The mixture was stirred at room temperature overnight. The organic layer was separated, washed with NaHC03 (200 mi x 3) and brine (200 ml), dried over anhydrous MgS04, concentrated and dried over vacuum to give the title compound. ‘H NMR (CDC13) : 5 5.20 (s, 2H); 4.44 (s, 4H); 1. 18 (s, 18H). 13c NMR (CDC13) : No. 153.3, 138.5, 117.3, 82.3, 66.9, 27.8.
In the field of chemistry, the synthetic routes of compounds are constantly being developed and updated. I will also mention this compound in other articles. 3513-81-3, 2-Methylenepropane-1,3-diol, other downstream synthetic routes, hurry up and to see.
Reference:
Patent; ENANTA PHARMACEUTICALS, INC.; WO2005/61526; (2005); A1;,
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