Related Products of 35106-82-2 ,Some common heterocyclic compound, 35106-82-2, molecular formula is C9H10O, its traditional synthetic route has been very mature, but the traditional synthetic route has various shortcomings, such as complicated route, low yield, poor purity, etc., below Introduce a new synthetic route.
General procedure: To a solution of the corresponding alkene (0.75 mmol) and (R)-1-phenylpent-4-en-3-ol (363 mg,2.2 mmol, 3.0 equiv) in CH2Cl2 (4 mL) was added Grubbs catalyst 2nd generation (6 mg, 7.5 mumol,0.01 equiv). The mixture was refluxed for 6 hours under an Ar atmosphere. After cooling, the reactionmixture was condensed its volume to 1 mL under the reduced pressure and the mixture wascharged directly on silica gel column chromatography to purify the corresponding cross-metathesisproduct.
These compound has a wide range of applications. It is believed that with the continuous development of the source of the synthetic route,35106-82-2, its application will become more common.
Reference:
Article; Ida, Akiko; Kitao, Kazuyuki; Hoshiya, Naoyuki; Uenishi, Jun’ichi; Tetrahedron Letters; vol. 56; 15; (2015); p. 1956 – 1959;,
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