In the next few decades, the world population will flourish. As the population grows rapidly and people all over the world use more and more resources, all industries must consider their environmental impact. 7073-69-0, name is 2-(2-Bromophenyl)propan-2-ol, the common compound, a new synthetic route is introduced below. Computed Properties of C9H11BrO
Using 2-norborneneA 10-mL dry sealed-tube equipped with a stir bar was charged with [RhCl(C2H4)2]2 (0.0125 mmol,4.86 mg), BIPHEP (0.0125 mmol, 6.53 mg), Li2CO3 (0.5 mmol, 36.9 mg), LiCl (0.1 mmol, 4.24 mg),and 2-norbornene (1.0 mmol, 94.1 mg) under a N2 flow. Xylene (1 mL), 2a (0.25 mmol, 53.8 mg),and furfural (0.5 mmol, 48.0 mg) were then added. After degassing the reaction mixture by the freezepump-thaw method three times, the tube was filled with N2. The mixture was then placed in an oilbath that had been preheated to 130 C for 20 h. After cooling to room temperature, the resultingsolution was filtered through a celite pad, and the filtrate was concentrated in vacuo. The resultingcrude product was purified by flash column chromatography on silica-gel to afford 6.
The synthetic route of 7073-69-0 has been constantly updated, and we look forward to future research findings.
Reference:
Article; Furusawa, Takuma; Tanimoto, Hiroki; Nishiyama, Yasuhiro; Morimoto, Tsumoru; Kakiuchi, Kiyomi; Chemistry Letters; vol. 46; 7; (2017); p. 926 – 929;,
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