Reference of 504-63-2, Adding some certain compound to certain chemical reactions, such as: 504-63-2, name is 1,3-Propanediol,molecular formula is C3H8O2, can increase the reaction rate and produce products with better performance than those obtained under traditional synthetic methods. Here is a downstream synthesis route of the compound 504-63-2.
General procedure: To a stirred solution of 2-naphthol (0.2 mmol) in TEAA(2 ml), was added acetic anhydride (0.22 mmol). The solutionwas stirred for 3 hours at room temperature. After consumptionof starting material (TLC monitoring, ethyl acetate/hexane, 2:8), the product formed was diluted with 1 mlH2O and extracted with 3 x 2 ml ether. The combined organiclayer was separated, dried (Na2SO4), and evaporatedunder reduced pressure to afford the desired product. 1H and13C NMR spectra were in full accordance with the structureproposed. The water in the aqueous layer was distilled under reduced pressure leaving behind the TEAA which was furtherrecycled.
According to the analysis of related databases, 504-63-2, the application of this compound in the production field has become more and more popular.
Reference:
Article; Lafuente, Leticia; Diaz, Gisela; Bravo, Rodolfo; Ponzinibbio, Agustin; Letters in Organic Chemistry; vol. 13; 3; (2016); p. 195 – 200;,
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