108-82-7, The major producers of chemicals have been the Europe, Japan and China. Due to the growing call for a cleaner, greener environment, people will have to find innovative ways to maintain their relevance. Here is a compound 108-82-7, name is 2,6-Dimethylheptan-4-ol. This compound has unique chemical properties. The synthetic route is as follows.
General procedure: NaOCl¡¤5H2O crystals (2.0 g, 12.2 mmol) were added in oneportion to a mixture of Bu4NHSO4 (0.17 g, 0.50 mmol),TEMPO (21 mg, 0.13 mmol), and 1 (1.30 g, 10.0 mmol) inCH2Cl2 (10 mL) at 5 C. After 15 min, GC monitoringshowed that 1 had been consumed. The reaction was stoppedafter 0.5 h by quenching with aq sat. Na2SO3 solution (20mL). The organic layer was separated, and the aqueous layerwas extracted with CH2Cl2 (30 mL). The combined organiclayers were washed with H2O (30 mL), dried over Na2SO4,and concentrated to give 2 as colorless oil (1.27 g, crudeyield of 99.2%, GC analysis showed the product to be 96.8%pure). A 0.42 g portion of the crude 2 was purified by bulbto-bulb distillation (6 kPa, 120-130 C) to afford pure 2(0.40 g, 95%). GC-MS analysis gave identical results tothose of an authentic sample.
While traditionally a conservative industry, chemical producers will need to modernize their PR strategies to stay relevant.we look forward to future research findings about 108-82-7, 2,6-Dimethylheptan-4-ol.
Reference:
Article; Okada, Tomohide; Asawa, Tomotake; Sugiyama, Yukihiro; Kirihara, Masayuki; Iwai, Toshiaki; Kimura, Yoshikazu; Synlett; vol. 25; 4; (2014); p. 596 – 598;,
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