Electric Literature of 769-30-2, Adding some certain compound to certain chemical reactions, such as: 769-30-2, name is Benzo[d][1,3]dioxol-4-ylmethanol,molecular formula is C8H8O3, can increase the reaction rate and produce products with better performance than those obtained under traditional synthetic methods. Here is a downstream synthesis route of the compound 769-30-2.
General procedure: A mixture of corresponding alcohol (1, 1 mmol) and 3,4-dihydro-2H-pyran (2, 100 mg, 1.2 mmol) was stirred in the presence of zwitterionic-salt A (10 mg, 10 mol%) at 60-80 C (oil bath) for 10-12 h in a seal tube. After completion of the reaction (TLC), the reaction mixture was cooled to room temperature and diluted with water (10 mL) and extracted with ethyl acetate (20 mL). Organic layer was dried over anhydrous Na2SO4. After evaporation of solvent the crude product was purified by column chromatography on silica gel using petroleum ether/ethyl acetate (4-5%) as eluent.
In the field of chemistry, the synthetic routes of compounds are constantly being developed and updated. I will also mention this compound in other articles. 769-30-2, Benzo[d][1,3]dioxol-4-ylmethanol, other downstream synthetic routes, hurry up and to see.
Reference:
Article; Mahato, Sachinta; Chatterjee, Rana; Chakraborty Ghosal, Nirnita; Majee, Adinath; Synthetic Communications; vol. 47; 20; (2017); p. 1905 – 1915;,
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