Application of 2568-33-4, As we all know, there are many different methods for the synthesis of a compound, and people can choose the synthesis method that suits their own laboratory according to the actual situation. 2568-33-4, name is 3-Methylbutane-1,3-diol, molecular formula is C5H12O2, The compound is widely used in many fields, so it is necessary to find a new synthetic route. The downstream synthesis method of this compound is introduced below.
To a cooled solution of 53 (2.0 g, 19.20 mmol, 1.0eq) in dichioromethane (40 mE) was added pyridine (3.03 g,38.4 mmol, 2.0 eq) followed by mesyl chloride (2.29 g,20.16 mmol, 1.05 eq) dropwise at 0 C. The reaction mixturewas stirred at room temperature for 1 h. After completion ofreaction, reaction mixture was transferred into ice cold waterand product was extracted with dichloro methane. Organic layer was combined, dried over sodium sulphate and concentrated under reduced pressure to obtain 53.1. (1.5 g, 42.86%), MS(ES): mlz 183.06 [M+H].
While traditionally a conservative industry, chemical producers will need to modernize their PR strategies to stay relevant.we look forward to future research findings about 2568-33-4, 3-Methylbutane-1,3-diol.
Reference:
Patent; Nimbus Lakshmi, Inc.; Masse, Craig E.; Greenwood, Jeremy Robert; Mondal, Sayan; Cowen, Scott D.; McLean, Thomas H.; (624 pag.)US2019/31664; (2019); A1;,
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