Synthetic Route of 23147-58-2, The major producers of chemicals have been the Europe, Japan and China. Due to the growing call for a cleaner, greener environment, people will have to find innovative ways to maintain their relevance. Here is a compound 23147-58-2, name is Glycerol aldehyde dimer. This compound has unique chemical properties. The synthetic route is as follows.
Glycol aldehyde dimer (1.0 g) was dissolved in demineralized water (14.5 g) . The solution was loaded into an autoclave along with 5% Ru on carbon catalyst (Sigma Aldrich, 0.20 g). The autoclave was purged 3 times with hydrogen and subsequently pressurized with hydrogen to the respective pressures given in Table 2. The mixture was heated to 80C from room temperature in the course of 15 min and stirred for 3 hours. The autoclave was then cooled to room temperature and the decrease in hydrogen pressure was noted.The product mixture was isolated from the catalyst by filtration and analyzed by HPLC and GC.Results of Examples 9 to 11 are provided in Table 4. The amount of 1, 2-butanediol (1,2-BDO) present in relation to ethylene glycol is provided. It can be seen that an increase in pressure of the reaction results in a reduction of 1,2-butanediol (1,2-BDO) formed, resulting in an increased purity of the ethylene glycol product in milder conditions.Table 4.
According to the analysis of related databases, 23147-58-2, the application of this compound in the production field has become more and more popular.
Reference:
Patent; HALDOR TOPSØE A/S; HOLM, Martin Spangsberg; TAARNING, Esben; (22 pag.)WO2016/1169; (2016); A1;,
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