Application of 30951-66-7, Adding some certain compound to certain chemical reactions, such as: 30951-66-7, name is 2-(3-Bromophenyl)propan-2-ol,molecular formula is C9H11BrO, can increase the reaction rate and produce products with better performance than those obtained under traditional synthetic methods. Here is a downstream synthesis route of the compound 30951-66-7.
11.1 [1-(3-Bromophenyl)-1-(methyl)ethyl]oxytrimethylsilane 3.4 g of the compound prepared according to 7.1 in 80 ml of dichloromethane, at 0 C., are placed in a round-bottomed flask. 5.6 ml of triethylamine and 4.5 ml of trimethylsilane chloride are added. The mixture is stirred for one hour at 0 C. and 20 h at ambient temperature. 50 ml of water are added and the mixture is extracted with 30 ml of dichloromethane. The organic phase is washed with 20 ml of a saturated solution of sodium chloride, dried over magnesium sulphate and then concentrated under reduced pressure. The residue is purified by silica gel chromatography, elution being carried out with a heptane/ethyl acetate mixture. 2.5 g of compound are obtained. 1H NMR (CDCl3, delta in ppm): 0 (s, 9H); 1.45 (s, 6H); 7.15 to 7.25 (m, 3H); 7.45 (m, 1H).
According to the analysis of related databases, 30951-66-7, the application of this compound in the production field has become more and more popular.
Reference:
Patent; SANOFI-AVENTIS; US2011/65727; (2011); A1;,
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