Adding a certain compound to certain chemical reactions, such as: 868594-48-3, 1-Phenyl-2,5,8,11,14,17,20,23,26-nonaoxaoctacosan-28-ol, can increase the reaction rate and produce products with better performance than those obtained under traditional synthetic methods. Here is a downstream synthesis route of the compound, Recommanded Product: 868594-48-3, blongs to alcohols-buliding-blocks compound. Recommanded Product: 868594-48-3
Compound d (0.684 g, 1.36 mmol, 2 eq) and triethylene glycol dimethanesulfonate (0.208 g, 0.68 mmol, 1 eq),Sodium hydroxide (116 mg, 2.9 mmol, 4.3eq) was added to a round flask, dissolved in 5 ml of tetrahydrofuran, stirred at room temperature for 12 hours, and then distilled under reduced pressure to dry the solvent.Thereafter, 87 mg of a palladium / carbon catalyst (Palladium on carbon) was added thereto, dissolved in 35 ml of ethanol, and stirred with hydrogen gas at room temperature for 12 hours.After distillation under reduced pressure, the solvent was dried and dichloromethane / methanol 9: 1 was purified by silica gel normal chromatography with a developing solution to obtain pure Compound A-2 (0.300 g, 39.3%)
At the same time, in my other blogs, there are other synthetic methods of this type of compound,868594-48-3, 1-Phenyl-2,5,8,11,14,17,20,23,26-nonaoxaoctacosan-28-ol, and friends who are interested can also refer to it.
Reference:
Patent; Bio Aekcheu Co., Ltd.; Park Jin-u; Jang Su-jeong; Lee Bong-gyu; Yoon Hyeong-jun; Song Mi-yeong; (13 pag.)KR102027694; (2019); B1;,
Alcohol – Wikipedia,
Alcohols – Chemistry LibreTexts