Researchers who often do experiments know that organic synthesis is a process of preparing more complex target molecules from simple raw materials through one or more chemical reactions. Generally, it requires fewer steps,and cheap raw materials. 5259-98-3, name is 5-Chloropentan-1-ol. A new synthetic method of this compound is introduced below., HPLC of Formula: C5H11ClO
General procedure: Compounds 2M-6M were prepared by a similar method. The synthesis of compound 6M is described below. 4,4?-Dihydroxydiphenyl (9.3 g, 0.05 mol) and 6-chloro-1-hexanol (15.1 g, 0.11 mol) were added to a solution of sodium hydroxide (4.4 g, 0.11 mol) in ethanol (200 mL, 95percent). The solution was heated to reflux for 20 h then was cooled and the solid salt was removed by filtration. The remaining solid was recrystallized from DMF/H2O to yield 15.6 g (81percent) of crystals.
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Reference:
Article; Chen, Cheng-Chih; Lin, Chih-Hung; Oriental Journal of Chemistry; vol. 34; 1; (2018); p. 125 – 133;,
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