Reference of 589-98-0, Adding some certain compound to certain chemical reactions, such as: 589-98-0, name is 3-Octanol,molecular formula is C8H18O, can increase the reaction rate and produce products with better performance than those obtained under traditional synthetic methods. Here is a downstream synthesis route of the compound 589-98-0.
General procedure: Compound 5 was dissolved in alcohol (13±16 equiv) and heated to 100C for 3 h in the presence of a catalytic amount of H2SO4 (0.1 equiv). Complete dissolution occurred while heating. The reaction was quenched by adding a saturated solution of NaHCO3 in water and the mixture was extracted with EtOAc. The organic layers were combined, and the solvent was evaporated under reducedpressure at 40C. The residual alcohol was removed by vacuum distillation. The crude residue was purified by flash column chromatography with appropriate eluents and a gradient. Diheptyl 2-[(4-methoxyphenoxy)methyl]pyrimidine-4,6-dicarboxylate (6a). Generalprocedure I was followed. Compound 5 (73 mg, 0.20 mmol), 1-heptanol (0.50 mL, 3.2 mmol,16 equiv), H2SO4 (1 muL, 0.03 mmol, 0.1 equiv). Flash chromatography eluents: n-hexane (A),Et2O (B); gradient: 8%66% B×10 CV. Compound 6a was isolated as a dark yellow oil (81mg, 0.16 mmol, 80% yield).
In the field of chemistry, the synthetic routes of compounds are constantly being developed and updated. I will also mention this compound in other articles. 589-98-0, 3-Octanol, other downstream synthetic routes, hurry up and to see.
Reference:
Article; Provenzani, Riccardo; Tarvainen, Ilari; Brandoli, Giulia; Lempinen, Antti; Artes, Sanna; Turku, Ainoleena; Jaentti, Maria Helena; Talman, Virpi; Yli-Kauhaluoma, Jari; Tuominen, Raimo K.; Boije af Gennaes, Gustav; PLoS ONE; vol. 13; 4; (2018);,
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