New learning discoveries about 702-98-7

While traditionally a conservative industry, chemical producers will need to modernize their PR strategies to stay relevant.we look forward to future research findings about 702-98-7, 2-Methyladamantan-2-ol.

702-98-7, Each compound has different characteristics, and only by selecting the characteristics of the compound suitable for a specific situation can the compound be applied on a large scale. 702-98-7, name is 2-Methyladamantan-2-ol. This compound has unique chemical properties. The synthetic route is as follows.

An autoclave was charged with 2,3-dibromo-1,1,1-trifluoropropane (0.2559 g, 1.0 mmol), 2-methyl-2-adamantanol (0.249 g, 1.5 mmol), triethylamine (0.202 g, 2.0 mmol), lithium carbonate(0.0369 g, 0.5 mmol), dichlorobis (triphenylphosphine) palladium(II) (0.0070 g, 0.01 mmol), and tetrahydrofuran (2.0 mL), which were then stirred at 100C for 15 hours after introducing carbon monoxide (1.0 MPaG). After the end of the reaction, the autoclave was cooled, ventilated, and added with benzotrifluoride as an internal standard substance, followed by stirring and leaving still for a while to let a salt precipitate. Quantification using a 19F-NMR integration value revealed that 2-trifluoromethyl acrylic acid 2-methyl-2-adamantyl ester was obtained with a yield of 91.1% on the basis of 2,3-dibromo-1,1,1-trifluoropropane.

While traditionally a conservative industry, chemical producers will need to modernize their PR strategies to stay relevant.we look forward to future research findings about 702-98-7, 2-Methyladamantan-2-ol.

Reference:
Patent; Tosoh F-Tech, Inc.; SAGAMI CHEMICAL RESEARCH CENTER; EP1637514; (2006); A1;,
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