Synthetic Route of 3391-86-4 , The common heterocyclic compound, 3391-86-4, name is Oct-1-en-3-ol, molecular formula is C8H16O, its traditional synthetic route has been very mature, but the traditional synthetic route has various shortcomings, such as complicated route, low yield, poor purity, etc., below Introduce a new synthetic route.
A solution of [Pd(HSS)] (1.25 × 10-7 to 2.5 × 10-7 mol) in water(100-200 muL), oct-1-en-3-ol (2.5 × 10-4 mol), and 3 mL of 0.2 Macetate buffer of appropriate pH (I = 0.2 M KCl) were placed into ahigh-pressure tube. The tube was repeatedly evacuated and filled withH2 and finally pressurized with H2 to reach 1-5 bar total pressure. Thereaction vessel was immersed into a thermostated bath (25-80 C), andthe mixture was stirred for the desired reaction time. At room temperaturethe products were extracted with 2 mL of toluene, dried overMgSO4, and subjected to gas chromatography.
The synthetic route of 3391-86-4 has been constantly updated, and we look forward to future research findings.
Reference:
Article; Lihi, Norbert; Bunda, Szilvia; Udvardy, Antal; Joo, Ferenc; Journal of Inorganic Biochemistry; vol. 203; (2020);,
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