Adding a certain compound to certain chemical reactions, such as: 6850-39-1, 3-Aminocyclohexanol, can increase the reaction rate and produce products with better performance than those obtained under traditional synthetic methods. Here is a downstream synthesis route of the compound, Recommanded Product: 6850-39-1, blongs to alcohols-buliding-blocks compound. Recommanded Product: 6850-39-1
To a stirred solution of 3-aminocyclohexanol (40.0 g, 0.348 mol) in DCM (350 ml) were added imidazole (71.0 g, 1.042 mol) and TBDMS-C1 (78.0 g, 0.520 mol) at 0 C. The mixture was allowed to stir at RT for 24 h. The reaction was quenched by H20, extracted with DCM, washed with brine solution, dried, filtered and concentrated to give title compound. Yield 78.1 g (crude); [M+H]+ = 230.
At the same time, in my other blogs, there are other synthetic methods of this type of compound,6850-39-1, 3-Aminocyclohexanol, and friends who are interested can also refer to it.
Reference:
Patent; ORION CORPORATION; WOHLFAHRT, Gerd; RUMMAKKO, Petteri; KARJALAINEN, Arja; PASSINIEMI, Mikko; PIETIKAeINEN, Pekka; HAIKARAINEN, Anssi; VAeISAeNEN, Emilia; TIAINEN, Eija; WO2014/202827; (2014); A1;,
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