Related Products of 15852-73-0, In the chemical reaction process,reaction time,type of solvent,can easily affect the result of the reaction, thereby determining the yield and properties of the reaction product.An updated downstream synthesis route of 15852-73-0 as follows.
General procedure: OMS-2-SH-B (20 mg, 10 mol%), benzyl alcohol (0.3 mmol) and benzamidine (0.5 mmol) were added into a Schlenk tube. Then, air was removed and toluene (1 mL) was added by a syringe under O2 atmosphere. If substituted benzyl alcohol was liquid, it was added with toluene under O2 balloon protection. If methyl benzene was used as substrate instead of benzyl alcohol, it was added as solvent (1 mL) into the reaction tube by syringe under O2 atmosphere. The mixture was stirred for required time at certain temperature for 20 h. The resulting mixture was cooled down, filtered and washed with EtOAc, and concentrated under reduced pressure to give the crude product. Finally, the product was purified by silica gel chromatography to yield the pure product.
These compound has a wide range of applications. It is believed that with the continuous development of the source of the synthetic route,15852-73-0, its application will become more common.
Reference:
Article; Shen, Jian; Meng, Xu; Catalysis Communications; vol. 127; (2019); p. 58 – 63;,
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