Analyzing the synthesis route of 7397-62-8

In the field of chemistry, the synthetic routes of compounds are constantly being developed and updated. I will also mention this compound in other articles. 7397-62-8, Butyl 2-hydroxyacetate, other downstream synthetic routes, hurry up and to see.

Synthetic Route of 7397-62-8, Adding some certain compound to certain chemical reactions, such as: 7397-62-8, name is Butyl 2-hydroxyacetate,molecular formula is C6H12O3, can increase the reaction rate and produce products with better performance than those obtained under traditional synthetic methods. Here is a downstream synthesis route of the compound 7397-62-8.

175.16 g (99%) of o-cresol and 214.10 g (99%) of n-butyl glycolate,And the catalyst Mo2P5-MCM-48 (Mo2P5 and MCM-48 mass ratio of 25:100) 1.32g was put into the reaction rectification apparatus, mixed and stirred, and the temperature was raised to 120 C, and the reaction was carried out for 3 hours.When the top of the column is substantially anhydrous, the reaction is completed, the temperature is lowered to room temperature, the catalyst is filtered off, and the filtrate is distilled to recover 64.85 g of o-cresol.a mixture of 48.94 g of n-butyl glycolate, 118.54 g,The product obtained n-butyl tolyloxyacetate 223.82g, purity 98.9%,The yield was 99.2% based on phenol.

In the field of chemistry, the synthetic routes of compounds are constantly being developed and updated. I will also mention this compound in other articles. 7397-62-8, Butyl 2-hydroxyacetate, other downstream synthetic routes, hurry up and to see.

Reference:
Patent; Shandong Runbo Biological Technology Co., Ltd.; Sun Guoqing; Hou Yongsheng; Chi Zhilong; Zhang Liguo; Hu Yishan; (13 pag.)CN108947839; (2018); A;,
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