New downstream synthetic route of (2,4-Dichlorophenyl)methanol

The synthetic route of 1777-82-8 has been constantly updated, and we look forward to future research findings.

Adding a certain compound to certain chemical reactions, such as: 1777-82-8, (2,4-Dichlorophenyl)methanol, can increase the reaction rate and produce products with better performance than those obtained under traditional synthetic methods. Here is a downstream synthesis route of the compound, Safety of (2,4-Dichlorophenyl)methanol, blongs to alcohols-buliding-blocks compound. Safety of (2,4-Dichlorophenyl)methanol

General procedure: Alcohol (1 mmol) was added to a mixture of MCM-41XANi(II) (0.03 g) and acetic anhydride (0.4 mL), and theresulting mixture was stirred at 50 C in solvent-free condition.After completion of the reaction (mentioned by TLC,ethylacetate: n-hexane, 3:7), dichloromethane (20 mL) wasadded and the catalyst was separated by filtration. Then, themixture was diluted with CH2Cl2.The organic phase washedwith 10% aqueous solution of sodium bicarbonate and driedover Na2SO4.Finally, the organic solvents were evaporatedand the product obtained with high to excellent yield.

The synthetic route of 1777-82-8 has been constantly updated, and we look forward to future research findings.

Reference:
Article; Nazarzadeh, Somayeh; Ghorbani-Choghamarani, Arash; Tahanpesar, Elham; Journal of the Iranian Chemical Society; vol. 15; 3; (2018); p. 649 – 659;,
Alcohol – Wikipedia,
Alcohols – Chemistry LibreTexts