Luzzio, Frederick A. published the artcilePreparation of β-phenylnitroethanes having electron-donating aryl substitution, Synthetic Route of 528594-30-1, the publication is Tetrahedron Letters (2007), 48(38), 6704-6708, database is CAplus.
β-Phenyl-β-hydroxynitroethanes having activating aryl substituents are treated with Et3SiH/F3CCO2H under solventless conditions to give the corresponding phenylnitroethanes. Substrates having no aryl substituents or substituents that are only mildly activating or deactivating do not result in appreciable conversion to the title compounds
Tetrahedron Letters published new progress about 528594-30-1. 528594-30-1 belongs to alcohols-buliding-blocks, auxiliary class Nitro Compound,Benzene,Phenol,Ether, name is 2-Methoxy-4-(2-nitroethyl)phenol, and the molecular formula is C9H11NO4, Synthetic Route of 528594-30-1.
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