Shimizu, Ken-ichi published the artcileSurface Oxygen-Assisted Pd Nanoparticle Catalysis for Selective Oxidation of Silanes to Silanols, SDS of cas: 597-52-4, the publication is Chemistry – A European Journal (2012), 18(8), 2226-2229, S2226/1-S2226/12, database is CAplus and MEDLINE.
Oxygen-adsorbed Pd surfaces show higher reactivity for water dissociation than clean Pd surfaces. Thus, carbon-supported Pd nanoparticles with surface oxygen atoms show higher activity for hydrolytic oxidation of silanes than previously reported catalysts. The synthetic utility of this catalyst is quite high because the catalyst, readily prepared from com. Pd/C, is easily recovered and reused, and shows high activity in oxidation of various silanes. This is a surface-science driven strategy of catalyst design for green organic synthesis. E.g., hydration of Et3SiH in presence of carbon-supported Pd nanoparticles covered with O gave >99% Et3SiOH, with TON = 20,000.
Chemistry – A European Journal published new progress about 597-52-4. 597-52-4 belongs to alcohols-buliding-blocks, auxiliary class Aliphatic Chain, name is Triethylsilanol, and the molecular formula is C4HN5, SDS of cas: 597-52-4.
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