Smolobochkin, A. V. published the artcileCyclization of 1-(4,4-diethoxybutyl)-3-aryl(thio)ureas to 2-arylpyrrolidines and 2,3′-bipyrrole derivatives, Quality Control of 6346-09-4, the publication is Russian Chemical Bulletin (2016), 65(3), 731-734, database is CAplus.
A reaction of 1-(4,4-diethoxybutyl)-3-phenylthiourea with resorcinol, 2-methylresorcinol, pyrogallol and hydroquinone in chloroform in the presence of trifluoroacetic acid leading to 2-aryl-1-(N-phenylcarbamothioyl)pyrrolidines I [R = H, Me, OH] and II has been described. The compounds such as 1-(4,4-diethoxybutyl)-3-aryl(thio)ureas R1NHC(X)NH(CH2)3CH(OC2H5)2 [R1 = C6H5, 4-H3COC6H4, 4-BrC6H4; X = O, S] in the presence of an acid catalyst undergo intramol. cyclization and dimerization with the formation of 1,1′-bis(N-arylcarbamo(thio)yl)-2,3′-bipyrrole derivatives III.
Russian Chemical Bulletin published new progress about 6346-09-4. 6346-09-4 belongs to alcohols-buliding-blocks, auxiliary class Amine,Aliphatic hydrocarbon chain,Ether, name is 4,4-Diethoxybutan-1-amine, and the molecular formula is C18H26ClN3O, Quality Control of 6346-09-4.
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