Brown, Alistair K. published the artcileValidated quantitative cannabis profiling for Canadian regulatory compliance – Cannabinoids, aflatoxins, and terpenes, Application In Synthesis of 124-76-5, the main research area is cannabinoid aflatoxin terpene determination LC MS cannabis; Aflatoxins; Cannabis; Chromatography; Mass spectrometry; Quantitative method; Terpenes.
In response to the Canadian federal government’s Cannabis Tracking and Licensing System compliance standards, a quant. method was created for cannabis anal., and validated using Eurachem V.2 (2014) guidelines. Cannabinol, cannabidiol, cannabigerol, cannabichromene, cannabidiolic acid, cannabigerolic acid, Δ-9-tetrahydrocannabinol, and Δ-9-tetrahydrocannabinolic acid A were all analyzed by scheduled multiple reaction monitoring (MRM) via LC-MS/MS and isotope dilution In addition, aflatoxins B1, B2, G1, and G2 were also analyzed by scheduled MRM via LC-MS/MS and matrix matched calibration curves to achieve the reporting limits (≤2μg kg-1) set out by the European Pharmacopoeia. The LODs/LOQs were 0.50/1.7, 2.0/6.7, 0.59/2.0, and 0.53/1.8μg kg-1, for B1, B2, G1, and G2 resp. Thirty one terpenes were analyzed by selected reaction monitoring via GC-MS/MS and isotope dilution using β-myrcene-d6 as a surrogate. All quant. analyses can be accomplished using less than 1 g of material, with minimal solvent and consumable use, on low resolution instruments in less than 30 min of instrument time. Of important note is this method’s power of selectivity, working ranges, and lack of need for extraction consumables such as SPE or QuEChERS, thereby minimising anal. costs and time.
Analytica Chimica Acta published new progress about Cannabinoids Role: ANT (Analyte), ANST (Analytical Study). 124-76-5 belongs to class alcohols-buliding-blocks, name is rel-(1R,2R,4R)-1,7,7-Trimethylbicyclo[2.2.1]heptan-2-ol, and the molecular formula is C10H18O, Application In Synthesis of 124-76-5.
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