Researchers who often do experiments know that organic synthesis is a process of preparing more complex target molecules from simple raw materials through one or more chemical reactions. Generally, it requires fewer steps,and cheap raw materials. 2807-30-9, name is 2-Propoxyethanol. A new synthetic method of this compound is introduced below., Application In Synthesis of 2-Propoxyethanol
10 g of the remaining bottoms of the distillation and 100 g of 2-n-propoxyethanol, 0.05 g of 4-pyrrolidinopyridine was charged into a reaction vessel equipped with a reflux condenser, Example 3 was carried out Distillation yielded 10 g of the preceding distillation and 123.8 g of thionyl chloride (Content 98.8%, sulfuryl chloride content 0.4%) were mixed,The stirring was started, and the mixture was slowly added dropwise to the reaction vessel. The procedure was as in Example 2. After completion of the dropping, heating was started, and the temperature was gradually raised to 98 C according to the reaction gas evolution rate.Until no gas release, continue to heat 4h get crude; The crude product was directly purified by distillation to obtain 116.41g of chloroethyl n-propyl ether. The product chromatogram was 99.2% and the water content was 0.15%. The yield was 98.9%.
If you are interested in these compounds, you can also browse my other articles.Thank you for taking the time to read this article. I hope you enjoyed it, 2807-30-9, 2-Propoxyethanol.
Reference:
Patent; Shandong Kaisheng New Materials Co.,Ltd.; Zhang, Taiming; Wang, Ronghai; Zhang, Qingxin; Zhang, Shanmin; Sun, Fengchun; Bi, Yixia; (6 pag.)CN105384612; (2016); A;,
Alcohol – Wikipedia,
Alcohols – Chemistry LibreTexts