Reference of 1611-56-9, Adding some certain compound to certain chemical reactions, such as: 1611-56-9, name is 11-Bromoundecan-1-ol,molecular formula is C11H23BrO, can increase the reaction rate and produce products with better performance than those obtained under traditional synthetic methods. Here is a downstream synthesis route of the compound 1611-56-9.
To a solution of 1-bromoundecanol 1 (30 g, 119.4 mmol) in DMF (150 ml_) was added NaN3 (15.5 g, 238.9 mmol) and the resulting mixture was stirred at 70 C for 12 h. The mixture was cooled to 23 C, filtered and the filtrate extracted with hexane (5 x 200 ml_). The hexanes fractions were combined and washed with H20 (2 x 100ml_), dried over anhydrous Na2S04 and concentrated under reduced pressure to afford 11-azidoundecan-1-ol 2 (24.19 g, 95%) as a colorless oil. 1H NMR (CDCI3) delta 3.62 (t, J = 6.6 Hz, 2H), 3.24 (t, J = 6.9 Hz, 2H), 1.61 -1.51 (m, 4H), 1.39-1.24 (m, 14H); 13C NMR (CDCI3) delta 63.15, 51.60, 32.89, 29.66, 29.56, 29.51 , 29.25, 28.95, 26.82, 25.84.
According to the analysis of related databases, 1611-56-9, the application of this compound in the production field has become more and more popular.
Reference:
Patent; RHODIA OPERATIONS; UNIVERSITY OF PENNSYLVANIA; CENTRE NATIONAL DE LA RECHERCHE SCIENTIFIQUE (C.N.R.S.); DONNIO, Bertrand; JISHKARIANI, Davit; DIROLL, Benjamin, T.; HOUGH, Lawrence; MURRAY, Christopher; CARGNELLO, Matteo; MALASSIS, Ludivine; (83 pag.)WO2016/201310; (2016); A1;,
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