Adding a certain compound to certain chemical reactions, such as: 23783-42-8, 2,5,8,11-Tetraoxatridecan-13-ol, can increase the reaction rate and produce products with better performance than those obtained under traditional synthetic methods. Here is a downstream synthesis route of the compound, 23783-42-8, blongs to alcohols-buliding-blocks compound. category: alcohols-buliding-blocks
To a stirred solution of triethyl amine (4.368 g, 40 mmol) and 2,5,8, 1 l-tetraoxatridecan-l3-ol (4.165 g, 20 mmol) in dichloromethane (30 mL) was added methanesulfonyl chloride (4.165 g, (0286) 20 mmol, diluted in 20 ml of dichloromethane) dropwise over 30 minutes at 0 C. The reaction was then stirred at room temperature overnight. Water (40 mL) was next added to the reaction. It was extracted with dichloromethane (3x 150 mL), and the organic phase was washed with 0.3 N HC1 (2×80 mL) and water (3 x 100 mL). After drying with NaiSOr. removal of the solvent provided the title compound (5.507 g, 96% yield). NMR (500 MHz, DMSO-riri) d: 4.33-4.29 (m, 2H), 3.70-3.64 (m, 2H), 3.59-3.49 (m, 10H), 3.45-3.42 (m, 2H), 3.24 (s, 3H), 3.17 (s, 3H).
These compound has a wide range of applications. It is believed that with the continuous development of the source of the synthetic route,23783-42-8, its application will become more common.
Reference:
Patent; ZHEJIANG VIMGREEN PHARMACEUTICALS, LTD; SUN, Sanxing; ZHAO, Long; HU, Chongbo; CHEN, Zhengshu; YE, Jinqi; (0 pag.)WO2020/2969; (2020); A1;,
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