Wang, Tianzhang published the artcileIntermolecular Multiple Dehydrogenative Cross-Couplings of Ketones with Boronic Acids and Amines via Copper Catalysis, Formula: C10H13NO2, the publication is Advanced Synthesis & Catalysis (2019), 361(16), 3886-3892, database is CAplus.
An intermol. multiple dehydrogenative coupling between ketones RC(O)CH2CH3 (R = Ph, thiophen-2-yl, (E)-2-phenylethenyl, etc.), cyclohexanone and nucleophilic amines NHR1R2 [R1 = H; R2 = Ph, pyridin-2-yl, morpholin-4-yl, etc.; R1R2 = (C2)2O(C2)2, (C2)5] or boronic acids ArB(OH)2 (Ar = Ph, furan-2-yl, anthracen-9-yl, etc.) using inexpensive copper(I) oxide as a catalyst was reported. This method provides a facile access to highly desirable chem. products such as α,β-unsaturated ketones (E)-RC(O)CH=CHAr, enaminones (E)-RC(O)CH=CHNR1R2, and synthetically relevant meta-substituted phenols R3C6H4OH (R3 = phenylaminyl, morpholin-4-yl, Ph, etc.).
Advanced Synthesis & Catalysis published new progress about 27292-49-5. 27292-49-5 belongs to alcohols-buliding-blocks, auxiliary class Morpholine,Benzene,Phenol, name is 3-Morpholinophenol, and the molecular formula is C9H12BNO4S, Formula: C10H13NO2.
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