Synthetic Route of 110-73-6, As we all know, there are many different methods for the synthesis of a compound, and people can choose the synthesis method that suits their own laboratory according to the actual situation. 110-73-6, name is 2-(Ethylamino)ethanol, molecular formula is C4H11NO, The compound is widely used in many fields, so it is necessary to find a new synthetic route. The downstream synthesis method of this compound is introduced below.
To a flask under a nitrogen atmosphere15 g (1 eq) of 4,4-difluorobenzophenone and 31.1 g of 2-ethylamino ethanol (5 eq) was added thereto,And the temperature was raised while stirring at 160 C.The reaction was carried out at 160 DEG C for 48 hours and then cooled to room temperature.Distilled water was added thereto, followed by extraction with methylene chloride or ethyl acetate, followed by drying under reduced pressure.The residue was recrystallized from ethyl acetate at room temperature to obtain an off-white Compound A. (20 g, 82% yield)
While traditionally a conservative industry, chemical producers will need to modernize their PR strategies to stay relevant.we look forward to future research findings about 110-73-6, 2-(Ethylamino)ethanol.
Reference:
Patent; LG CHEM, LTD.; Lee, Dami; Park, Jong-Ho; (30 pag.)KR2017/3170; (2017); A;,
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