Application of 1777-82-8, As we all know, there are many different methods for the synthesis of a compound, and people can choose the synthesis method that suits their own laboratory according to the actual situation. 1777-82-8, name is (2,4-Dichlorophenyl)methanol, molecular formula is C7H6Cl2O, The compound is widely used in many fields, so it is necessary to find a new synthetic route. The downstream synthesis method of this compound is introduced below.
General procedure: Catalytic experiments were carried out in a 5-mL test tube. In a typical procedure, to 1 mmol benzyl alcohol in 1 ml solvent, 2 mol% (0.02 g) of gamma-Fe2O3-MoO2L and 2 mmolof 30 % H2O2 was added. The reaction mixture was stirred for 3 h at 80 C. The reaction products were monitored byTLC or GC. After completion of the reaction, the mixture was diluted with EtOAc. The catalyst was separated by an external magnet, washed with EtOAc, dried and reused for a consecutive run under the same reaction conditions. Evaporation of the solvent from the filtrate under reduced pressure gave the crude products, which were then purified by chromatography on silica gel eluted with n-hexane/EtOAc (2:1).
According to the analysis of related databases, 1777-82-8, the application of this compound in the production field has become more and more popular.
Reference:
Article; Saeednia; Ardakani, M. Hatefi; Parizi, Z. Pakdin; Hafshejani, M. Tavakoli; Transition Metal Chemistry; vol. 41; 7; (2016); p. 767 – 774;,
Alcohol – Wikipedia,
Alcohols – Chemistry LibreTexts