Araujo, Yara Jaqueline Kerber published the artcileSynthesis and enzymatic resolution of racemic 2,3-epoxy propyl esters obtained from glycerol, Application In Synthesis of 57044-25-4, the publication is Tetrahedron Letters (2015), 56(13), 1696-1698, database is CAplus.
A method is described for the synthesis of (±)-2,3-epoxy Pr esters from glycerol, involving reaction of epichlorohydrin with sodium or potassium salts of carboxylic acids in the presence of TBAB as catalyst, with moderate to excellent yields. Kinetic resolution of glycidyl butyrate by lipase of Thermomyces lanuginosa has been achieved with remarkable enantiomeric excess (ee >99%) using 1,4-dioxane as a co-solvent in pure buffer solution (30 and 50 °C, pH = 7.0).
Tetrahedron Letters published new progress about 57044-25-4. 57044-25-4 belongs to alcohols-buliding-blocks, auxiliary class Epoxides,Chiral,Aliphatic hydrocarbon chain,Alcohol, name is (R)-Oxiran-2-ylmethanol, and the molecular formula is C3H6O2, Application In Synthesis of 57044-25-4.
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