Ford, Russell L. published the artcileIntramolecular Pd-Catalyzed Reductive Amination of Enolizable sp3-C-H Bonds, Product Details of C7H6FNO3, the publication is Organic Letters (2019), 21(21), 8827-8831, database is CAplus and MEDLINE.
A palladium-catalyzed reductive cyclization of nitroarenes has been designed to construct sp3-C-NHAr bonds from sp3-C-H bonds by using an enolizable nucleophile to intercept a nitrosoarene intermediate. Exposure of ortho-substituted nitroarenes to 5 mol % of Pd(OAc)2 and 10 mol % of phenanthroline under 2 atm of CO constructs partially saturated 5-, 6-, or 7-membered N-heterocycles I (R1 = H, Cl, Me, etc.; R2 = H, F, Me, etc.; R3 = H, Me) using α-pyridyl carboxylates, malonates, 1,3-dimethylbarbituric acid, 1,3-diones, or difurans as the nucleophile.
Organic Letters published new progress about 1043416-40-5. 1043416-40-5 belongs to alcohols-buliding-blocks, auxiliary class Fluoride,Nitro Compound,Benzene,Alcohol, name is (4-Fluoro-2-nitrophenyl)methanol, and the molecular formula is C7H6FNO3, Product Details of C7H6FNO3.
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