Synthetic Route of 756520-66-8, Researchers who often do experiments know that organic synthesis is a process of preparing more complex target molecules from simple raw materials through one or more chemical reactions. Generally, it requires fewer steps,and cheap raw materials. 756520-66-8, name is 1-(2,6-Dichloro-3-fluorophenyl)ethanol. A new synthetic method of this compound is introduced below.
A solution of 1- (2,6-dichloro-3-fluorophenyl) ethanol (5 g, 23.9 mmol) in hydrobromic acid (30 ml) When cooled to room temperature. Extracted with ethyl acetate. The combined organic phases were washed with water, dried over anhydrous sodium sulfate and concentrated to give the product (5.2 g, Yield: 80%).
At the same time, in my other blogs, there are other synthetic methods of this type of compound,756520-66-8, 1-(2,6-Dichloro-3-fluorophenyl)ethanol, and friends who are interested can also refer to it.
Reference:
Patent; Tianjin Binjiang Pharmaceutical Inc.; Tian, Hongqi; Huang, Gongchao; (33 pag.)CN103497177; (2017); B;,
Alcohol – Wikipedia,
Alcohols – Chemistry LibreTexts