On June 30, 1984, Osman, Fayez H.; Gawad, Mahfouz M. Abdel; Abbasi, Mohamed M. published an article.Application In Synthesis of 2,2′-(tert-Butylazanediyl)diethanol The title of the article was The behavior of N-tert-butyl-2,2′-iminodiethanol towards some trivalent phosphorus compounds. And the article contained the following:
Treating (HOCH2CH2)2NCMe3 (I) with PCl3 or HMPT in C6H6 gave the 2:3 adduct II, which was hydrolyzed by H2O to give the dioxazaphosphocane oxide III (R = H) (IV) and I. Treating IV with o-chloranil gave a crystalline product which in solution gave an equilibrium mixture of V (R = OH) and III (R = OC6Cl4OH-2). PhPCl2 or (Me2N)2PPh reacted with I to give dioxazaphosphocane VI, which added o-chloranil to give an equilibrium mixture of VII and V (R = Ph). Treating VI with PhN3 gave the imine VIII. The experimental process involved the reaction of 2,2′-(tert-Butylazanediyl)diethanol(cas: 2160-93-2).Application In Synthesis of 2,2′-(tert-Butylazanediyl)diethanol
The Article related to dioxazaphosphocane derivative, iminodiethanol cyclization phosphorus compound, butyliminodiethanol cyclization phosphorus compound, Organometallic and Organometalloidal Compounds: Phosphorus Compounds and other aspects.Application In Synthesis of 2,2′-(tert-Butylazanediyl)diethanol
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