Application of 629-30-1, Researchers who often do experiments know that organic synthesis is a process of preparing more complex target molecules from simple raw materials through one or more chemical reactions. Generally, it requires fewer steps,and cheap raw materials. 629-30-1, name is 1,7-Heptanediol. A new synthetic method of this compound is introduced below.
Fe(NO3)3¡¤9H2O (40.4 mg, 10 molpercent) and ABNO (7 mg, 5 molpercent) were used in this order.1,7-heptanediol (132 mg, 1 mmol) was added to a 10 ml reaction tube.Then add 2ml of acetonitrile as a solvent and open the reaction at room temperature.The degree of reaction was then checked by GC-MS. Reaction 15h,After the reaction is over,An internal standard, n-dodecane, was added and the product was quantitatively analyzed by GC.1,7-heptanediol conversion rate of 86percent,Product yield 85percent.
At the same time, in my other blogs, there are other synthetic methods of this type of compound,629-30-1, 1,7-Heptanediol, and friends who are interested can also refer to it.
Reference:
Patent; Dalian Institute of Chemical Physics; Gao Shuang; Wang Lianyue; Chen Bo; Lv Ying; (5 pag.)CN106831675; (2017); A;,
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