Adding a certain compound to certain chemical reactions, such as: 35106-82-2, (2-Vinylphenyl)methanol, can increase the reaction rate and produce products with better performance than those obtained under traditional synthetic methods. Here is a downstream synthesis route of the compound, 35106-82-2, blongs to alcohols-buliding-blocks compound. name: (2-Vinylphenyl)methanol
Step 3: (1,3-dihydroisobenzofuran-1-yl)methanol To a mixture of (2-vinylphenyl)methanol (obtained from step 2) (1.0 g, 7.45 mmol) in DCM (10 mL) was added m-CPBA (1.82 g, 8.94 mmol) in small portions at 0¡ã C. The reaction mixture was stirred at room temperature for overnight, and then the mixture was diluted with DCM (30 mL) and washed with saturated NaHCO3 aqueous solution and brine. The organic layer was dried over sodium sulfate and concentrated under vacuum. The residue was purified by prep-TLC (petroleum ether:ethyl acetate=4:1) to afford (1,3-dihydroisobenzofuran-1-yl) methanol (260 mg, yield: 23percent) as yellow oil. m/z: [M+H]+ 151.1
These compound has a wide range of applications. It is believed that with the continuous development of the source of the synthetic route,35106-82-2, its application will become more common.
Reference:
Patent; SHANGHAI DE NOVO PHARMATECH CO. LTD.; GAO, Daxin; YANG, Heping; WANG, Pei; (84 pag.)US2017/37038; (2017); A1;,
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