Gibka, Julia’s team published research in Zeszyty Naukowe – Politechnika Lodzka, Chemia Spozywcza i Biotechnologia in 2004 | CAS: 58783-82-7

Zeszyty Naukowe – Politechnika Lodzka, Chemia Spozywcza i Biotechnologia published new progress about Acetalization. 58783-82-7 belongs to class alcohols-buliding-blocks, name is 5-Tridecanol, and the molecular formula is C13H28O, Synthetic Route of 58783-82-7.

Gibka, Julia published the artcileDerivatives of tridecan-X-ones (X = 2-7): Synthesis and spectral data, Synthetic Route of 58783-82-7, the main research area is tridecanone diol acetalization; acetal tridecanone preparation; dioxolane preparation; dioxane preparation; tridecyl acetate preparation.

Tridecan-x-ones (x = 2-7) have been used as starting materials in the synthesis of ethylene and propylene acetals, tridecan-x-ols and their acetates. Cyclic acetals were obtained in the reaction between ketone and ethane-1,2-diol or propane-1,2-diol in toluene in the presence of sulfosalicylic acid as a catalyst. Alcs. were synthesized in the reduction of ketones with sodium borohydride in water/2-propanol. Acetates were prepared by the esterification of alcs. with acetic anhydride in the presence of sodium acetate. All derivatives were prepared in a 2-5 g scale. Phys. properties (b.p., refractive index, elemental anal.) and spectral data (IR, 1H NMR) for all the synthesized derivatives of tridecan-x-ones have been determined

Zeszyty Naukowe – Politechnika Lodzka, Chemia Spozywcza i Biotechnologia published new progress about Acetalization. 58783-82-7 belongs to class alcohols-buliding-blocks, name is 5-Tridecanol, and the molecular formula is C13H28O, Synthetic Route of 58783-82-7.

Referemce:
Alcohol – Wikipedia,
Alcohols – Chemistry LibreTexts