Klunder, Janice M. published the artcileArenesulfonate derivatives of homochiral glycidol: versatile chiral building blocks for organic synthesis, COA of Formula: C6H9N3O2S, the publication is Journal of Organic Chemistry (1989), 54(6), 1295-304, database is CAplus.
The preparation of a series of crystalline arenesulfonate derivatives of enantiomerically enriched glycidol is described. The enhancement of optical purity by recrystallization was particularly successful for two of these derivatives, glycidyl tosylate and glycidyl 3-nitrobenzenesulfonate, which were obtained in 97% ee and 99% ee, resp. Very high regioselectivity was observed in the reactions of these compounds with a variety of nucleophiles, including aryl oxides, Et2AlCN, organometallic reagents, and BH3-NaBH4. The application of this methodol. to the synthesis of homochiral β-adrenergic blocking agents and homochiral terminal epoxides is discussed.
Journal of Organic Chemistry published new progress about 30165-97-0. 30165-97-0 belongs to alcohols-buliding-blocks, auxiliary class Morpholine,Thiadiazole,Alcohol, name is 4-Morpholino-1,2,5-thiadiazol-3-ol, and the molecular formula is C6H9N3O2S, COA of Formula: C6H9N3O2S.
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