Wang, Dungai published the artcileLiBr-Catalyzed C3-Disulfuration between Indole and N-Dithiophthalimide, Recommanded Product: 2-Phenylethanethiol, the publication is Journal of Organic Chemistry, database is CAplus and MEDLINE.
A simple, green halide-catalyzed protocol for disulfuration of indole derivatives with N-dithiophthalimides was developed. This C-H disulfide reaction proceeded smoothly at room temperature with economical LiBr as catalyst, providing an effective method for the synthesis of novel unsym. disulfides. A series of 3-dithioindole derivatives were obtained in high yields with good functional group tolerance, moreover, the wide scope of Harpp reagents (aryl, benzyl, primary, secondary, tertiary) confirmed the practicability of this approach.
Journal of Organic Chemistry published new progress about 4410-99-5. 4410-99-5 belongs to alcohols-buliding-blocks, auxiliary class Thiol,Benzene, name is 2-Phenylethanethiol, and the molecular formula is C2H2N4O2, Recommanded Product: 2-Phenylethanethiol.
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