Steiman, Talia J. published the artcileSynthesis of β-Phenethylamines via Ni/Photoredox Cross-Electrophile Coupling of Aliphatic Aziridines and Aryl Iodides, Recommanded Product: 2-Aminobutan-1-ol, the publication is Journal of the American Chemical Society (2020), 142(16), 7598-7605, database is CAplus and MEDLINE.
A photoassisted Ni-catalyzed reductive cross-coupling between tosyl-protected alkyl aziridines and com. available (hetero)aryl iodides is reported. This mild and modular method proceeds in the absence of stoichiometric heterogeneous reductants and uses an inexpensive organic photocatalyst to access medicinally valuable β-phenethylamine derivatives Unprecedented reactivity was achieved with the activation of cyclic aziridines. Mechanistic studies suggest that the regioselectivity and reactivity observed under these conditions are a result of nucleophilic iodide ring opening of the aziridine to generate an iodoamine as the active electrophile. This strategy also enables cross-coupling with Boc-protected aziridines.
Journal of the American Chemical Society published new progress about 96-20-8. 96-20-8 belongs to alcohols-buliding-blocks, auxiliary class Amine,Aliphatic hydrocarbon chain,Alcohol, name is 2-Aminobutan-1-ol, and the molecular formula is C7H7ClN2S, Recommanded Product: 2-Aminobutan-1-ol.
Referemce:
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