Mamat, Marhaba published the artcileA visible-light-induced thiol addition/aerobic oxidation cascade reaction of epoxides and thiols for the synthesis of β-hydroxylsulfoxides, Safety of 2-Phenylethanethiol, the publication is Organic & Biomolecular Chemistry (2021), 19(45), 9855-9859, database is CAplus and MEDLINE.
A photochem. thiol addition/aerobic oxidation cascade reaction had been developed. This protocol enabled efficient oxidative coupling of epoxides and thiols to access structurally valuable β-hydroxylsulfoxides RSO2CH2C(R1R2)OH [R = 4-MeC6H4, 4-ClC6H4, 4-MeOC6H4, etc.; R1 = H, Me; R2 = Me, Et, CO2Et, etc.]. A broad range of functional groups were compatible to obtain moderate to good yields of the target products. Mechanistic studies revealed a sequential reaction pathway involving base-promoted thiol addition of thiols to epoxides and visible-light-induced aerobic oxygenation of thioethers.
Organic & Biomolecular Chemistry published new progress about 4410-99-5. 4410-99-5 belongs to alcohols-buliding-blocks, auxiliary class Thiol,Benzene, name is 2-Phenylethanethiol, and the molecular formula is C8H10S, Safety of 2-Phenylethanethiol.
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